2-[3-(2-{2-[2-(tert-butoxycarbonylamino)ethoxy]ethoxy}ethoxy)-prop-1-ynyl]-2',3'-O-isopropylidene-5'-O-[N-(n-tetradecanoyl)sulfamoyl]adenosine triethylammonium salt

Base Information

Chemical Name:2-[3-(2-{2-[2-(tert-butoxycarbonylamino)ethoxy]ethoxy}ethoxy)-prop-1-ynyl]-2',3'-O-isopropylidene-5'-O-[N-(n-tetradecanoyl)sulfamoyl]adenosine triethylammonium salt
CAS No.:1333880-69-5
Molecular Formula:C₆H₁₅N*C₄₁H₆₇N₇O₁₂S
Molecular Weight:983.28
Hs Code.:

2-[3-(2-{2-[2-(tert-butoxycarbonylamino)ethoxy]ethoxy}ethoxy)-prop-1-ynyl]-2',3'-O-isopropylidene-5'-O-[N-(n-tetradecanoyl)sulfamoyl]adenosine triethylammonium salt

Synonyms:2-[3-(2-{2-[2-(tert-butoxycarbonylamino)ethoxy]ethoxy}ethoxy)-prop-1-ynyl]-2',3'-O-isopropylidene-5'-O-[N-(n-tetradecanoyl)sulfamoyl]adenosine triethylammonium salt

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Chemical Property of 2-[3-(2-{2-[2-(tert-butoxycarbonylamino)ethoxy]ethoxy}ethoxy)-prop-1-ynyl]-2',3'-O-isopropylidene-5'-O-[N-(n-tetradecanoyl)sulfamoyl]adenosine triethylammonium salt

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Technology Process of 2-[3-(2-{2-[2-(tert-butoxycarbonylamino)ethoxy]ethoxy}ethoxy)-prop-1-ynyl]-2',3'-O-isopropylidene-5'-O-[N-(n-tetradecanoyl)sulfamoyl]adenosine triethylammonium salt

There total 1 articles about 2-[3-(2-{2-[2-(tert-butoxycarbonylamino)ethoxy]ethoxy}ethoxy)-prop-1-ynyl]-2',3'-O-isopropylidene-5'-O-[N-(n-tetradecanoyl)sulfamoyl]adenosine triethylammonium salt which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 77.0%

: 69888-86-4
N-succinimidyl myristate

: 1333880-67-3
2-[3-(2-{2-[2-(tert-butoxycarbonylamino)ethoxy]ethoxy}ethoxy)prop-1-ynyl]-2',3'-O-isopropylidene-5'-O-(sulfamoyl)adenosine

: 121-44-8
triethylamine

: 1333880-69-5
2-[3-(2-{2-[2-(tert-butoxycarbonylamino)ethoxy]ethoxy}ethoxy)-prop-1-ynyl]-2',3'-O-isopropylidene-5'-O-[N-(n-tetradecanoyl)sulfamoyl]adenosine triethylammonium salt

Guidance literature:: N-succinimidyl myristate; 2-[3-(2-{2-[2-(tert-butoxycarbonylamino)ethoxy]ethoxy}ethoxy)prop-1-ynyl]-2',3'-O-isopropylidene-5'-O-(sulfamoyl)adenosine; With caesium carbonate; In N,N-dimethyl-formamide; at 0 - 23 ℃; for 16h; Inert atmosphere;

triethylamine; In methanol; ethyl acetate; flash chromatography;
DOI:10.1016/j.ab.2011.06.037