1,2',6'-tri-N-tert-butoxycarbonyl-2''-N-formimidoylistamycin B hydrochloride

Base Information

Chemical Name:1,2',6'-tri-N-tert-butoxycarbonyl-2''-N-formimidoylistamycin B hydrochloride
CAS No.:81202-85-9
Molecular Formula:C₃₃H₆₀N₆O₁₁*ClH
Molecular Weight:753.334
Hs Code.:

Synonyms:1,2',6'-tri-N-tert-butoxycarbonyl-2''-N-formimidoylistamycin B hydrochloride

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Chemical Property of 1,2',6'-tri-N-tert-butoxycarbonyl-2''-N-formimidoylistamycin B hydrochloride

Chemical Property:

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Technology Process of 1,2',6'-tri-N-tert-butoxycarbonyl-2''-N-formimidoylistamycin B hydrochloride

There total 5 articles about 1,2',6'-tri-N-tert-butoxycarbonyl-2''-N-formimidoylistamycin B hydrochloride which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 38.0%

: 16694-46-5
ethyl formimidate hydrochloride

: 1,2',6'-tri-N-tert-butoxycarbonylistamycin B acetate

: 81202-85-9
1,2',6'-tri-N-tert-butoxycarbonyl-2''-N-formimidoylistamycin B hydrochloride

Guidance literature:: In methanol; for 4h; Ambient temperature;
DOI:10.1016/0008-6215(82)84028-7

Reference yield:

: 58632-95-4
2-(tert-Butoxycarbonyloxyimino)-2-phenylacetonitrile

: 81202-85-9
1,2',6'-tri-N-tert-butoxycarbonyl-2''-N-formimidoylistamycin B hydrochloride

Guidance literature:: Multi-step reaction with 4 steps

1: 49 percent / Zn(OAc)2*2H₂O / methanol / Ambient temperature

2: 94 percent / Et₃N / dioxane / 2 h / 60 °C

3: 237 mg / H₂ / 5percent Pd-C / methanol; acetic acid; H₂O / 3 h

4: 38 percent / methanol / 4 h / Ambient temperature

With zinc diacetate; hydrogen; triethylamine; palladium on activated charcoal; In 1,4-dioxane; methanol; water; acetic acid;
DOI:10.1016/0008-6215(82)84028-7

Reference yield:

: 77312-49-3
1,2',6'-tri-N-tert-butoxycarbonylistamycin B₀

: 81202-85-9
1,2',6'-tri-N-tert-butoxycarbonyl-2''-N-formimidoylistamycin B hydrochloride

Guidance literature:: Multi-step reaction with 3 steps

1: 94 percent / Et₃N / dioxane / 2 h / 60 °C

2: 237 mg / H₂ / 5percent Pd-C / methanol; acetic acid; H₂O / 3 h

3: 38 percent / methanol / 4 h / Ambient temperature

With hydrogen; triethylamine; palladium on activated charcoal; In 1,4-dioxane; methanol; water; acetic acid;
DOI:10.1016/0008-6215(82)84028-7