N-Boc-3-O-benzyl-(2S,3S)-2-amino-3,5-dihydroxyvaleric acid tert-butyl ester

Base Information

• Chemical Name: N-Boc-3-O-benzyl-(2S,3S)-2-amino-3,5-dihydroxyvaleric acid tert-butyl ester
• CAS No.: 1206532-49-1
• Molecular Formula: C₂₁H₃₃NO₆
• Molecular Weight: 395.496

Synonyms:N-Boc-3-O-benzyl-(2S,3S)-2-amino-3,5-dihydroxyvaleric acid tert-butyl ester

Chemical Property of N-Boc-3-O-benzyl-(2S,3S)-2-amino-3,5-dihydroxyvaleric acid tert-butyl ester

Chemical Property:

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Technology Process of N-Boc-3-O-benzyl-(2S,3S)-2-amino-3,5-dihydroxyvaleric acid tert-butyl ester

There total 1 articles about N-Boc-3-O-benzyl-(2S,3S)-2-amino-3,5-dihydroxyvaleric acid tert-butyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

C21H31NO6 → N-Boc-3-O-benzyl-(2S,3S)-2-amino-3,5-dihydroxyvaleric acid tert-butyl ester (1206532-49-1)

Guidance literature:

With sodium tetrahydroborate; In methanol; at 0 - 20 ℃;

DOI:10.1016/j.tet.2009.10.102

Reference yield: 73.0%

N-Boc-3-O-benzyl-(2S,3S)-2-amino-3,5-dihydroxyvaleric acid tert-butyl ester (1206532-49-1) + N,N’,N’’-tri(benzyloxycarbonyl)guanidine (216584-23-5) → N2-Boc-N5,N7,N7'-tris-Cbz-3-O-benzyl-(3S)-3-hydroxy-L-arginine tert-butyl ester (1206532-50-4)

Guidance literature:

With di-isopropyl azodicarboxylate; triphenylphosphine; In tetrahydrofuran; at 0 - 20 ℃;

DOI:10.1016/j.tet.2009.10.102

Downstream raw materials:

N₂-Boc-N₅,N₇,N₇'-tris-Cbz-3-O-benzyl-(3S)-3-hydroxy-L-arginine tert-butyl ester

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