Technology Process of C29H28O11
There total 4 articles about C29H28O11 which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
With
ethanol; toluene-4-sulfonic acid;
In
dichloromethane;
at 55 ℃;
for 5h;
Inert atmosphere;
DOI:10.1016/j.cclet.2016.03.017
- Guidance literature:
-
Multi-step reaction with 3 steps
1: lithium aluminium tetrahydride / tetrahydrofuran / 0 °C / Reflux; Inert atmosphere
2: triphenylphosphine; di-isopropyl azodicarboxylate / tetrahydrofuran / 0 - 50 °C / Inert atmosphere
3: pyridinium p-toluenesulfonate / dichloromethane; ethanol / 4 h / 55 °C / Inert atmosphere
With
lithium aluminium tetrahydride; di-isopropyl azodicarboxylate; pyridinium p-toluenesulfonate; triphenylphosphine;
In
tetrahydrofuran; ethanol; dichloromethane;
2: |Mitsunobu Displacement;
DOI:10.1002/chem.201301385
- Guidance literature:
-
Multi-step reaction with 2 steps
1: triphenylphosphine; di-isopropyl azodicarboxylate / tetrahydrofuran / 0 - 50 °C / Inert atmosphere
2: pyridinium p-toluenesulfonate / dichloromethane; ethanol / 4 h / 55 °C / Inert atmosphere
With
di-isopropyl azodicarboxylate; pyridinium p-toluenesulfonate; triphenylphosphine;
In
tetrahydrofuran; ethanol; dichloromethane;
1: |Mitsunobu Displacement;
DOI:10.1002/chem.201301385