Technology Process of Benzyl-((R)-1-ethyl-4-oxo-undecyl)-carbamic acid benzyl ester
There total 9 articles about Benzyl-((R)-1-ethyl-4-oxo-undecyl)-carbamic acid benzyl ester which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
With
4 A molecular sieve; pyridinium chlorochromate;
In
dichloromethane;
Ambient temperature;
DOI:10.1016/S0040-4039(00)99129-9
- Guidance literature:
-
Multi-step reaction with 7 steps
1: NaOH / H2O; dioxane / 5 °C
2: Me2SO, (COCl)2, Et3N / CH2Cl2 / -78 °C
3: tetrahydrofuran / Ambient temperature
4: 85 percent / NaBH4, LiCl / ethanol; tetrahydrofuran / Ambient temperature
5: 97 percent / PCC, molecular sieves 4 Angstroem / CH2Cl2 / Ambient temperature
6: 92 percent / diethyl ether / Ambient temperature
7: 95 percent / PCC, molecular sieves 4 Angstroem / CH2Cl2 / Ambient temperature
With
sodium hydroxide; sodium tetrahydroborate; oxalyl dichloride; 4 A molecular sieve; dimethyl sulfoxide; triethylamine; pyridinium chlorochromate; lithium chloride;
In
tetrahydrofuran; 1,4-dioxane; diethyl ether; ethanol; dichloromethane; water;
DOI:10.1016/S0040-4039(00)99129-9
- Guidance literature:
-
Multi-step reaction with 2 steps
1: 92 percent / diethyl ether / Ambient temperature
2: 95 percent / PCC, molecular sieves 4 Angstroem / CH2Cl2 / Ambient temperature
With
4 A molecular sieve; pyridinium chlorochromate;
In
diethyl ether; dichloromethane;
DOI:10.1016/S0040-4039(00)99129-9
