N-(2,4-dimethoxy-benzyl),N-(ethyl ethanylat-2-yl)-5-aminomethyl-3-phenyl-isothiazole-4-carboxylic acid methyl ester

Base Information

Chemical Name:N-(2,4-dimethoxy-benzyl),N-(ethyl ethanylat-2-yl)-5-aminomethyl-3-phenyl-isothiazole-4-carboxylic acid methyl ester
CAS No.:1172590-68-9
Molecular Formula:C₂₅H₂₈N₂O₆S
Molecular Weight:484.573
Hs Code.:

Synonyms:N-(2,4-dimethoxy-benzyl),N-(ethyl ethanylat-2-yl)-5-aminomethyl-3-phenyl-isothiazole-4-carboxylic acid methyl ester

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Chemical Property of N-(2,4-dimethoxy-benzyl),N-(ethyl ethanylat-2-yl)-5-aminomethyl-3-phenyl-isothiazole-4-carboxylic acid methyl ester

Chemical Property:

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Technology Process of N-(2,4-dimethoxy-benzyl),N-(ethyl ethanylat-2-yl)-5-aminomethyl-3-phenyl-isothiazole-4-carboxylic acid methyl ester

There total 1 articles about N-(2,4-dimethoxy-benzyl),N-(ethyl ethanylat-2-yl)-5-aminomethyl-3-phenyl-isothiazole-4-carboxylic acid methyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1172590-68-9
N-(2,4-dimethoxy-benzyl),N-(ethyl ethanylat-2-yl)-5-aminomethyl-3-phenyl-isothiazole-4-carboxylic acid methyl ester

Guidance literature:

Reference yield:

: 1172590-68-9
N-(2,4-dimethoxy-benzyl),N-(ethyl ethanylat-2-yl)-5-aminomethyl-3-phenyl-isothiazole-4-carboxylic acid methyl ester

: 1172589-44-4
6-(2,4-dimethoxy-benzyl)-4-oxo-3-phenyl-4,5,6,7-tetrahydro-isothiazolo[5,4-c]pyridine-5-carboxylic acid ethyl ester

Guidance literature:: With potassium tert-butylate; In tetrahydrofuran; at -78 - 20 ℃; for 2.5h; Product distribution / selectivity;

Reference yield:

: 1172590-68-9
N-(2,4-dimethoxy-benzyl),N-(ethyl ethanylat-2-yl)-5-aminomethyl-3-phenyl-isothiazole-4-carboxylic acid methyl ester

: 1172589-47-7
7-(4-fluoro-phenyl)-4-hydroxy-3-phenyl-isothiazolo[5,4-c]pyridine-5-carboxylic acid ethyl ester

Guidance literature:: Multi-step reaction with 4 steps

1: potassium tert-butylate / tetrahydrofuran / 2.5 h / -78 - 20 °C

2: thionyl chloride / dichloromethane / 3 h / 20 °C

3: N-Bromosuccinimide; dibenzoyl peroxide / tetrachloromethane / 4 h / Reflux

4: bis-triphenylphosphine-palladium(II) chloride / N,N-dimethyl-formamide / 0.5 h / 120 °C

With N-Bromosuccinimide; thionyl chloride; potassium tert-butylate; dibenzoyl peroxide; bis-triphenylphosphine-palladium(II) chloride; In tetrahydrofuran; tetrachloromethane; dichloromethane; N,N-dimethyl-formamide;