Laudanosine-6'-carboxylic acid

Base Information

Chemical Name:Laudanosine-6'-carboxylic acid
CAS No.:62067-26-9
Molecular Formula:C₂₂H₂₇NO₆
Molecular Weight:401.459
Hs Code.:

Synonyms:Laudanosine-6'-carboxylic acid

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Chemical Property of Laudanosine-6'-carboxylic acid

Chemical Property:

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Technology Process of Laudanosine-6'-carboxylic acid

There total 5 articles about Laudanosine-6'-carboxylic acid which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 100.0%

: 50461-22-8
6'-Laudanosincarbonsaeuremethylester

: 62067-26-9
Laudanosine-6'-carboxylic acid

Guidance literature:: With potassium hydroxide; for 1h; Heating;
DOI:10.1002/ardp.19823150312

Reference yield: 70.0%

: 50461-20-6
6'-Hydroxymethyl-laudanosine

: 67928-50-1
6'-Formyllaudanosin

: 62067-26-9
Laudanosine-6'-carboxylic acid

Guidance literature:: With dipyridinium dichromate; In N,N-dimethyl-formamide; for 10h; Ambient temperature;
DOI:10.1002/ardp.19823150312

Reference yield:

: 50461-20-6
6'-Hydroxymethyl-laudanosine

: 62067-26-9
Laudanosine-6'-carboxylic acid

Guidance literature:: Multi-step reaction with 3 steps

1: 80 percent / PDC / CH₂Cl₂ / 10 h / Ambient temperature

2: 1.) NaCN, glacial acetic acid, 2.) MnO₂ / 1.) room temp., 3 h, 2.) room temp., 12 h; reflux, 10 h

3: 100 percent / 20percent aq. KOH / 1 h / Heating

With manganese(IV) oxide; potassium hydroxide; dipyridinium dichromate; sodium cyanide; acetic acid; In dichloromethane;
DOI:10.1002/ardp.19823150312