O-benzyldalbergin

Base Information

Chemical Name:O-benzyldalbergin
CAS No.:934815-44-8
Molecular Formula:C₂₃H₁₈O₄
Molecular Weight:358.394
Hs Code.:

Synonyms:O-benzyldalbergin

Suppliers and Price of O-benzyldalbergin

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of O-benzyldalbergin

Chemical Property:

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Technology Process of O-benzyldalbergin

There total 8 articles about O-benzyldalbergin which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 77.0%

: 934815-40-4
C₂₃H₂₀O₃

: 934815-44-8
O-benzyldalbergin

Guidance literature:: With 2,3-dicyano-5,6-dichloro-p-benzoquinone; In 1,4-dioxane; at 20 ℃; for 1h;
DOI:10.1016/j.tetlet.2007.01.117

Reference yield:

: 934815-37-9
C₂₄H₂₂O₄

: 934815-44-8
O-benzyldalbergin

Guidance literature:: Multi-step reaction with 3 steps

1: 88 percent / tert-BuOK

2: 96 percent / Grubbs' catalyst (II) / CH₂Cl₂ / 8 h / 20 °C

3: 77 percent / DDQ / dioxane / 1 h / 20 °C

With potassium tert-butylate; 2,3-dicyano-5,6-dichloro-p-benzoquinone; Grubbs' catalyst (II); In 1,4-dioxane; dichloromethane; 1: Wittig reaction;
DOI:10.1016/j.tetlet.2007.01.117

Reference yield:

: 934815-38-0
C₂₅H₂₄O₃

: 934815-44-8
O-benzyldalbergin

Guidance literature:: Multi-step reaction with 2 steps

1: 96 percent / Grubbs' catalyst (II) / CH₂Cl₂ / 8 h / 20 °C

2: 77 percent / DDQ / dioxane / 1 h / 20 °C

With 2,3-dicyano-5,6-dichloro-p-benzoquinone; Grubbs' catalyst (II); In 1,4-dioxane; dichloromethane;
DOI:10.1016/j.tetlet.2007.01.117