[4-(4,7-dihydro-1-thia-4,5-diazacyclopenta[a]pentalen-6-yl)phenyl]pyridin-3-ylamine hydrochloride

Base Information

• Chemical Name: [4-(4,7-dihydro-1-thia-4,5-diazacyclopenta[a]pentalen-6-yl)phenyl]pyridin-3-ylamine hydrochloride
• CAS No.: 1469858-74-9
• Molecular Formula: C₁₉H₁₄N₄S*ClH
• Molecular Weight: 366.874

Synonyms:[4-(4,7-dihydro-1-thia-4,5-diazacyclopenta[a]pentalen-6-yl)phenyl]pyridin-3-ylamine hydrochloride

Chemical Property of [4-(4,7-dihydro-1-thia-4,5-diazacyclopenta[a]pentalen-6-yl)phenyl]pyridin-3-ylamine hydrochloride

Chemical Property:

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Technology Process of [4-(4,7-dihydro-1-thia-4,5-diazacyclopenta[a]pentalen-6-yl)phenyl]pyridin-3-ylamine hydrochloride

There total 7 articles about [4-(4,7-dihydro-1-thia-4,5-diazacyclopenta[a]pentalen-6-yl)phenyl]pyridin-3-ylamine hydrochloride which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 80.0%

pyridin-3-yl-{4-[4-(2-trimethylsilanylethoxymethyl)-4,7-dihydro-1-thia-4,5-diazacyclopenta[a]pentalen-6-yl]phenyl}amine (1469858-44-3) → [4-(4,7-dihydro-1-thia-4,5-diazacyclopenta[a]pentalen-6-yl)phenyl]pyridin-3-ylamine hydrochloride (1469858-74-9)

Guidance literature:

With hydrogenchloride; In methanol; at 100 ℃; for 4h;

Reference yield: 80.0%

C25H28N4O2SSi → [4-(4,7-dihydro-1-thia-4,5-diazacyclopenta[a]pentalen-6-yl)phenyl]pyridin-3-ylamine hydrochloride (1469858-74-9)

Guidance literature:

With hydrogenchloride; In methanol; water; at 100 ℃; for 4h;

Reference yield:

6-(4-bromophenyl)-4-(2-trimethylsilanylethoxymethyl)-4,7-dihydro-1-thia-4,5-diazacyclopenta[a]pentalene (1469858-10-3) → [4-(4,7-dihydro-1-thia-4,5-diazacyclopenta[a]pentalen-6-yl)phenyl]pyridin-3-ylamine hydrochloride (1469858-74-9)

Guidance literature:

Multi-step reaction with 2 steps

1: caesium carbonate; palladium diacetate; 4,5-bis(diphenylphosphino)-9,9-dimethylxanthene / 1,4-dioxane / 8 h / 100 °C

2: hydrogenchloride / methanol / 4 h / 100 °C

With hydrogenchloride; palladium diacetate; caesium carbonate; 4,5-bis(diphenylphosphino)-9,9-dimethylxanthene; In 1,4-dioxane; methanol;

upstream raw materials:

6-(4-bromophenyl)-4,7-dihydro-1-thia-4,5-diazacyclopenta[a]pentalene

6-(4-bromophenyl)-4-(2-trimethylsilanylethoxymethyl)-4,7-dihydro-1-thia-4,5-diazacyclopenta[a]pentalene

pyridin-3-yl-{4-[4-(2-trimethylsilanylethoxymethyl)-4,7-dihydro-1-thia-4,5-diazacyclopenta[a]pentalen-6-yl]phenyl}amine

5,6-dihydro-<6H>-cyclopenta--thiophene-4-one

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