Technology Process of 3,67-trimethylocta-2,6-dienyl bromide
There total 1 articles about 3,67-trimethylocta-2,6-dienyl bromide which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
Multi-step reaction with 5 steps
1.1: potassium carbonate / acetone / Inert atmosphere; Reflux
2.1: potassium hydroxide / ethanol; water / 3.5 h / Inert atmosphere; Reflux
3.1: diisopropylamine; n-butyllithium / tetrahydrofuran; hexane / 1 h / -78 - 0 °C / Inert atmosphere
3.2: 20 °C / Inert atmosphere
4.1: diisobutylaluminium hydride / hexane; diethyl ether / 1 h / 20 °C / Inert atmosphere
5.1: phosphorus tribromide / 1.5 h / 0 - 20 °C / Inert atmosphere
With
n-butyllithium; phosphorus tribromide; diisobutylaluminium hydride; potassium carbonate; diisopropylamine; potassium hydroxide;
In
tetrahydrofuran; diethyl ether; ethanol; hexane; water; acetone;
DOI:10.1002/chem.202100962
- Guidance literature:
-
Multi-step reaction with 2 steps
1: potassium carbonate / acetone / Inert atmosphere; Reflux
2: potassium hydroxide / ethanol; water / 3.5 h / Inert atmosphere; Reflux
With
potassium carbonate; potassium hydroxide;
In
ethanol; water; acetone;
DOI:10.1002/chem.202100962
