(2aR,4S,4aS,7aS,7bS)-7-benzyl-7b-methoxy-4-(phenylthio)hexahydro-2H,4H-1,3,6-trioxa-7-azacyclopenta[cd]indene

Base Information

Chemical Name:(2aR,4S,4aS,7aS,7bS)-7-benzyl-7b-methoxy-4-(phenylthio)hexahydro-2H,4H-1,3,6-trioxa-7-azacyclopenta[cd]indene
CAS No.:1257939-01-7
Molecular Formula:C₂₁H₂₃NO₄S
Molecular Weight:385.484
Hs Code.:

Synonyms:(2aR,4S,4aS,7aS,7bS)-7-benzyl-7b-methoxy-4-(phenylthio)hexahydro-2H,4H-1,3,6-trioxa-7-azacyclopenta[cd]indene

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Chemical Property of (2aR,4S,4aS,7aS,7bS)-7-benzyl-7b-methoxy-4-(phenylthio)hexahydro-2H,4H-1,3,6-trioxa-7-azacyclopenta[cd]indene

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Technology Process of (2aR,4S,4aS,7aS,7bS)-7-benzyl-7b-methoxy-4-(phenylthio)hexahydro-2H,4H-1,3,6-trioxa-7-azacyclopenta[cd]indene

There total 1 articles about (2aR,4S,4aS,7aS,7bS)-7-benzyl-7b-methoxy-4-(phenylthio)hexahydro-2H,4H-1,3,6-trioxa-7-azacyclopenta[cd]indene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 59.0%

: 1257939-03-9
(3S,4'S)-2-benzyl-3-(2-phenylthio-[1,3]dioxolan-4-yl)-4-methoxy-3,6-dihydro-2H-[1,2]-oxazine

: 1257939-01-7
(2aR,4S,4aS,7aS,7bS)-7-benzyl-7b-methoxy-4-(phenylthio)hexahydro-2H,4H-1,3,6-trioxa-7-azacyclopenta[cd]indene

Guidance literature:: With trimethylsilyl trifluoromethanesulfonate; In dichloromethane; at -30 - 20 ℃; for 16h; Inert atmosphere;
DOI:10.1002/chem.201001060

Reference yield: 53.0%

: 1257939-01-7
(2aR,4S,4aS,7aS,7bS)-7-benzyl-7b-methoxy-4-(phenylthio)hexahydro-2H,4H-1,3,6-trioxa-7-azacyclopenta[cd]indene

: 583040-99-7
4-methoxyphenyl 2,3-O-isopropylidene-α-L-rhamnopyranoside

: 1257939-16-4
C₃₁H₃₉NO₁₀

Guidance literature:: With N-iodo-succinimide; In dichloromethane; at 20 ℃; for 1h; Molecular sieve; Inert atmosphere;
DOI:10.1002/chem.201001060