C₂₀H₂₃NO₇

Base Information

Chemical Name:C₂₀H₂₃NO₇
CAS No.:1562377-58-5
Molecular Formula:C₂₀H₂₃NO₇
Molecular Weight:389.405
Hs Code.:

C<sub>20</sub>H<sub>23</sub>NO<sub>7</sub>

Synonyms:C₂₀H₂₃NO₇

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Chemical Property of C₂₀H₂₃NO₇

Chemical Property:

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Technology Process of C₂₀H₂₃NO₇

There total 5 articles about C₂₀H₂₃NO₇ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1562377-54-1
C₁₈H₂₅NO₃

: 1562377-58-5
C₂₀H₂₃NO₇

: 1562377-60-9
C₂₀H₂₃NO₇

Guidance literature:: Multi-step reaction with 2 steps

1.1: potassium hexamethylsilazane / tetrahydrofuran / 0.08 h / -78 °C / Molecular sieve; Inert atmosphere

1.2: 5 h / -78 - 20 °C / Molecular sieve; Inert atmosphere

2.1: benzene / 12 h / 150 °C / Sealed tube; Inert atmosphere

With potassium hexamethylsilazane; In tetrahydrofuran; benzene;
DOI:10.1021/ol4034447

Reference yield:

: 1562377-48-3
C₁₄H₂₀BrNO₄

: 1562377-58-5
C₂₀H₂₃NO₇

: 1562377-60-9
C₂₀H₂₃NO₇

Guidance literature:: Multi-step reaction with 5 steps

1.1: iodoform; samarium / tetrahydrofuran / Inert atmosphere; Reflux

1.2: 3 h / 0 °C / Inert atmosphere

2.1: potassium hexamethylsilazane; N,N,N,N,N,N-hexamethylphosphoric triamide / tetrahydrofuran / 1 h / -78 °C / Inert atmosphere

2.2: 18 h / -78 - 20 °C / Inert atmosphere

3.1: potassium hexamethylsilazane; N,N,N,N,N,N-hexamethylphosphoric triamide / tetrahydrofuran / 1 h / -78 °C / Inert atmosphere

3.2: 18 h / -78 - 20 °C / Inert atmosphere

4.1: potassium hexamethylsilazane / tetrahydrofuran / 0.08 h / -78 °C / Molecular sieve; Inert atmosphere

4.2: 5 h / -78 - 20 °C / Molecular sieve; Inert atmosphere

5.1: benzene / 12 h / 150 °C / Sealed tube; Inert atmosphere

With N,N,N,N,N,N-hexamethylphosphoric triamide; samarium; iodoform; potassium hexamethylsilazane; In tetrahydrofuran; benzene;
DOI:10.1021/ol4034447

Reference yield:

: 1562377-50-7
C₁₄H₁₉NO₃

: 1562377-58-5
C₂₀H₂₃NO₇

: 1562377-60-9
C₂₀H₂₃NO₇

Guidance literature:: Multi-step reaction with 4 steps

1.1: potassium hexamethylsilazane; N,N,N,N,N,N-hexamethylphosphoric triamide / tetrahydrofuran / 1 h / -78 °C / Inert atmosphere

1.2: 18 h / -78 - 20 °C / Inert atmosphere

2.1: potassium hexamethylsilazane; N,N,N,N,N,N-hexamethylphosphoric triamide / tetrahydrofuran / 1 h / -78 °C / Inert atmosphere

2.2: 18 h / -78 - 20 °C / Inert atmosphere

3.1: potassium hexamethylsilazane / tetrahydrofuran / 0.08 h / -78 °C / Molecular sieve; Inert atmosphere

3.2: 5 h / -78 - 20 °C / Molecular sieve; Inert atmosphere

4.1: benzene / 12 h / 150 °C / Sealed tube; Inert atmosphere

With N,N,N,N,N,N-hexamethylphosphoric triamide; potassium hexamethylsilazane; In tetrahydrofuran; benzene;
DOI:10.1021/ol4034447