[N(P(C₆H₅)3)2]⁽¹⁺⁾*[Pt(C₆F₅)2Cl(CO)]^(1-)=[N(P(C₆H₅)3)2][Pt(C₆F₅)2Cl(CO)]

Base Information

Chemical Name:[N(P(C₆H₅)3)2]⁽¹⁺⁾*[Pt(C₆F₅)2Cl(CO)]^(1-)=[N(P(C₆H₅)3)2][Pt(C₆F₅)2Cl(CO)]
CAS No.:102779-25-9
Molecular Formula:C₁₃ClF₁₀OPt*C₃₆H₃₀NP₂
Molecular Weight:1131.25
Hs Code.:

[N(P(C<sub>6</sub>H<sub>5</sub>)3)2]<sup>(1+)</sup>*[Pt(C<sub>6</sub>F<sub>5</sub>)2Cl(CO)]<sup>(1-)</sup>=[N(P(C<sub>6</sub>H<sub>5</sub>)3)2][Pt(C<sub>6</sub>F<sub>5</sub>)2Cl(CO)]

Synonyms:[N(P(C₆H₅)3)2]⁽¹⁺⁾*[Pt(C₆F₅)2Cl(CO)]^(1-)=[N(P(C₆H₅)3)2][Pt(C₆F₅)2Cl(CO)]

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Chemical Property of [N(P(C₆H₅)3)2]⁽¹⁺⁾*[Pt(C₆F₅)2Cl(CO)]^(1-)=[N(P(C₆H₅)3)2][Pt(C₆F₅)2Cl(CO)]

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Technology Process of [N(P(C₆H₅)3)2]⁽¹⁺⁾*[Pt(C₆F₅)2Cl(CO)]^(1-)=[N(P(C₆H₅)3)2][Pt(C₆F₅)2Cl(CO)]

There total 4 articles about [N(P(C₆H₅)3)2]⁽¹⁺⁾*[Pt(C₆F₅)2Cl(CO)]^(1-)=[N(P(C₆H₅)3)2][Pt(C₆F₅)2Cl(CO)] which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 93.0%

: cis-[Pt(C₆F₅)2(CO)2]

: 21050-13-5
bis(triphenylphosphine)iminium chloride

: 102779-25-9
[N(P(C₆H₅)3)2]⁽¹⁺⁾*[Pt(C₆F₅)2Cl(CO)]^(1-)=[N(P(C₆H₅)3)2][Pt(C₆F₅)2Cl(CO)]

Guidance literature:: In dichloromethane; byproducts: CO; inert atmosphere; addn. of (PPN)Cl to soln. of Pt-complex, stirring; evapn. to dryness, dissoln. in CH2Cl2, slow diffusion of hexane (-30°C); elem. anal.;
DOI:10.1021/om00139a012

Reference yield: 86.0%

: 2(C₆H₅)3PNP(C₆H₅)3⁽¹⁺⁾*{(C₆F₅)2Pt(Cl)2Pt(C₆F₅)2}^(2-)=(N(P(C₆H₅)3)2)2{Pt₂Cl₂(C₆F₅)4}

: 102779-25-9
[N(P(C₆H₅)3)2]⁽¹⁺⁾*[Pt(C₆F₅)2Cl(CO)]^(1-)=[N(P(C₆H₅)3)2][Pt(C₆F₅)2Cl(CO)]

Guidance literature:: With CO; In dichloromethane; inert atmosphere; passing CO through soln. of Pt-complex (room temp., 10 min); evapn. to dryness, dissoln. in 2-PrOH, layering with hexane (crystn.); elem. anal.;
DOI:10.1021/om00139a012

Reference yield:

: tetrabutylammonium trans-bis(pentafluorophenyl)(carbony)(Cl)platinum(II)

: 102779-25-9
[N(P(C₆H₅)3)2]⁽¹⁺⁾*[Pt(C₆F₅)2Cl(CO)]^(1-)=[N(P(C₆H₅)3)2][Pt(C₆F₅)2Cl(CO)]

Guidance literature:: Multi-step reaction with 3 steps

1: CO / tetrahydrofuran

2: neat (no solvent)

3: dichloromethane

With CO; In tetrahydrofuran; dichloromethane;
DOI:10.1021/om00139a012