sodium ((3aS,5R,6R,6aS)-6-(benzyloxy)-2,2-dimethyltetrahydrofuro[2,3-d][1,3]dioxol-5-yl)methyl sulphate

Base Information

Chemical Name:sodium ((3aS,5R,6R,6aS)-6-(benzyloxy)-2,2-dimethyltetrahydrofuro[2,3-d][1,3]dioxol-5-yl)methyl sulphate
CAS No.:1607447-47-1
Molecular Formula:C₁₅H₁₉O₈S*Na
Molecular Weight:382.367
Hs Code.:

Synonyms:sodium ((3aS,5R,6R,6aS)-6-(benzyloxy)-2,2-dimethyltetrahydrofuro[2,3-d][1,3]dioxol-5-yl)methyl sulphate

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Chemical Property of sodium ((3aS,5R,6R,6aS)-6-(benzyloxy)-2,2-dimethyltetrahydrofuro[2,3-d][1,3]dioxol-5-yl)methyl sulphate

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Technology Process of sodium ((3aS,5R,6R,6aS)-6-(benzyloxy)-2,2-dimethyltetrahydrofuro[2,3-d][1,3]dioxol-5-yl)methyl sulphate

There total 5 articles about sodium ((3aS,5R,6R,6aS)-6-(benzyloxy)-2,2-dimethyltetrahydrofuro[2,3-d][1,3]dioxol-5-yl)methyl sulphate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 90.0%

: 19139-80-1,34370-91-7,68354-70-1,70798-12-8,59358-33-7
((3aS,5R,6R,6aS)-6-(benzyloxy)-2,2-dimethyltetrahydrofuro[2,3-d][1,3]dioxol-5-yl)methanol

: 1607447-47-1
sodium ((3aS,5R,6R,6aS)-6-(benzyloxy)-2,2-dimethyltetrahydrofuro[2,3-d][1,3]dioxol-5-yl)methyl sulphate

Guidance literature:: With sulfur trioxide pyridine complex; In N,N-dimethyl-formamide; for 1h;
DOI:10.1016/j.carres.2014.01.004

Reference yield:

: 168103-00-2
(((3aS,5R,6R,6aS)-6-(benzyloxy)-2,2-dimethyltetrahydrofuro[2,3-d][1,3]dioxol-5-yl)methoxy)(tert-butyl)diphenylsilane

: 1607447-47-1
sodium ((3aS,5R,6R,6aS)-6-(benzyloxy)-2,2-dimethyltetrahydrofuro[2,3-d][1,3]dioxol-5-yl)methyl sulphate

Guidance literature:: Multi-step reaction with 2 steps

1: tetrabutyl ammonium fluoride / tetrahydrofuran / 1 h

2: sulfur trioxide pyridine complex / N,N-dimethyl-formamide / 1 h

With tetrabutyl ammonium fluoride; sulfur trioxide pyridine complex; In tetrahydrofuran; N,N-dimethyl-formamide;
DOI:10.1016/j.carres.2014.01.004

Reference yield:

: 532-20-7,613-83-2,7261-25-8,7687-39-0,13221-22-2,14795-83-6,15761-67-8,20074-49-1,25545-03-3,25545-04-4,32445-75-3,34436-17-4,36441-93-7,36468-53-8,37110-85-3,37388-49-1,38029-69-5,40461-77-6,40461-89-0,41546-19-4,41546-20-7,41546-21-8,41546-26-3,41546-29-6,41546-30-9,41546-31-0,126872-16-0,131064-98-7
D-arabinofuranose

: 1607447-47-1
sodium ((3aS,5R,6R,6aS)-6-(benzyloxy)-2,2-dimethyltetrahydrofuro[2,3-d][1,3]dioxol-5-yl)methyl sulphate

Guidance literature:: Multi-step reaction with 5 steps

1: pyridine / 0 - 4 °C / Inert atmosphere

2: camphor-10-sulfonic acid / dichloromethane / 4 °C / Inert atmosphere

3: sodium hydride / 3 h / 20 °C

4: tetrabutyl ammonium fluoride / tetrahydrofuran / 1 h

5: sulfur trioxide pyridine complex / N,N-dimethyl-formamide / 1 h

With pyridine; camphor-10-sulfonic acid; tetrabutyl ammonium fluoride; sulfur trioxide pyridine complex; sodium hydride; In tetrahydrofuran; dichloromethane; N,N-dimethyl-formamide;
DOI:10.1016/j.carres.2014.01.004