trop2PPh

Base Information

• Chemical Name: trop2PPh
• CAS No.: 1204348-65-1
• Molecular Formula: C₃₆H₂₇P
• Molecular Weight: 490.584

Synonyms:trop2PPh

Chemical Property of trop2PPh

Chemical Property:

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Technology Process of trop2PPh

There total 2 articles about trop2PPh which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 84.0%

5H-dibenzo[a,d]cyclohepten-5-yl chloride + phenylphosphane (638-21-1) → trop2PPh (1204348-65-1)

Guidance literature:

With 1,4-diaza-bicyclo[2.2.2]octane; In toluene; Inert atmosphere; Reflux;

DOI:10.1002/anie.200903201

Reference yield: 84.0%

5-chloro-5H-dibenzo[a,d]cycloheptene (18506-04-2) + phenylphosphane (638-21-1) → trop2PPh (1204348-65-1)

Guidance literature:

With 1,4-diaza-bicyclo[2.2.2]octane; In toluene; Inert atmosphere; Reflux;

DOI:10.1021/ja909022p

Reference yield: 94.0%

tetrahydrofuran (109-99-9,24979-97-3,77392-70-2) + chloro(1,5-cyclooctadiene)rhodium(I) dimer + trop2PPh (1204348-65-1) → Rh2(mu.-Cl)2[(5H-dibenzo[a,d]-cyclohepten-5-yl)2PPh]2*1.5C4H8O

Guidance literature:

In tetrahydrofuran; Rh complex and trop2PPh dissolved in THF; stirred for 1 d at 298 K;

DOI:10.1002/anie.200903201

upstream raw materials:

phenylphosphane

5-chloro-5H-dibenzo[a,d]cycloheptene

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