isopropyl 2-{[3,5-bis(trifluoromethyl)phenyl]sulfonyl}-5-methyl-2-(3-methylbut-2-enyl)hex-4-enoate

Base Information

Chemical Name:isopropyl 2-{[3,5-bis(trifluoromethyl)phenyl]sulfonyl}-5-methyl-2-(3-methylbut-2-enyl)hex-4-enoate
CAS No.:533889-38-2
Molecular Formula:C₂₃H₂₈F₆O₄S
Molecular Weight:514.529
Hs Code.:

Synonyms:isopropyl 2-{[3,5-bis(trifluoromethyl)phenyl]sulfonyl}-5-methyl-2-(3-methylbut-2-enyl)hex-4-enoate

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Chemical Property of isopropyl 2-{[3,5-bis(trifluoromethyl)phenyl]sulfonyl}-5-methyl-2-(3-methylbut-2-enyl)hex-4-enoate

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Technology Process of isopropyl 2-{[3,5-bis(trifluoromethyl)phenyl]sulfonyl}-5-methyl-2-(3-methylbut-2-enyl)hex-4-enoate

There total 4 articles about isopropyl 2-{[3,5-bis(trifluoromethyl)phenyl]sulfonyl}-5-methyl-2-(3-methylbut-2-enyl)hex-4-enoate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 99.0%

: 870-63-3
prenyl bromide

: 404825-83-8
isopropyl {[3,5-bis(trifluoromethyl)phenyl]sulfonyl}acetate

: 533889-38-2
isopropyl 2-{[3,5-bis(trifluoromethyl)phenyl]sulfonyl}-5-methyl-2-(3-methylbut-2-enyl)hex-4-enoate

Guidance literature:: With pyridine; In dichloromethane; at -80 - 16 ℃; for 3h;
DOI:10.1023/A:1020363826262

Reference yield:

: 29921-57-1
isopropyl 2-bromoacetate

: 533889-38-2
isopropyl 2-{[3,5-bis(trifluoromethyl)phenyl]sulfonyl}-5-methyl-2-(3-methylbut-2-enyl)hex-4-enoate

Guidance literature:: Multi-step reaction with 3 steps

1: 99 percent / NaH / acetonitrile / 24 h / 20 °C

2: 92 percent / oxone / methanol; H₂O / 24 h / 20 °C

3: 78 percent / K₂CO₃; Bu₄NBr / acetonitrile / 24 h / 20 °C

With Oxone; tetrabutylammomium bromide; sodium hydride; potassium carbonate; In methanol; water; acetonitrile;
DOI:10.1002/hlca.200290013

Reference yield:

: 130783-02-7
3,5-bis(trifluoromethyl)thiophenol

: 533889-38-2
isopropyl 2-{[3,5-bis(trifluoromethyl)phenyl]sulfonyl}-5-methyl-2-(3-methylbut-2-enyl)hex-4-enoate

Guidance literature:: Multi-step reaction with 3 steps

1: 99 percent / NaH / acetonitrile / 24 h / 20 °C

2: 92 percent / oxone / methanol; H₂O / 24 h / 20 °C

3: 78 percent / K₂CO₃; Bu₄NBr / acetonitrile / 24 h / 20 °C

With Oxone; tetrabutylammomium bromide; sodium hydride; potassium carbonate; In methanol; water; acetonitrile;
DOI:10.1002/hlca.200290013