Technology Process of C25H17N
There total 5 articles about C25H17N which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
With
tetrakis(triphenylphosphine) palladium(0); sodium formate; N-ethyl-N,N-diisopropylamine;
In
acetonitrile;
at 60 ℃;
for 4h;
Inert atmosphere;
DOI:10.1055/s-0030-1259556
- Guidance literature:
-
Multi-step reaction with 4 steps
1: copper(l) iodide; tetrakis(triphenylphosphine) palladium(0); tetrabutylammomium bromide; triethylamine / N,N-dimethyl-formamide / Heating
2: pyridine; hydroxylamine hydrochloride / Heating
3: triethylamine / dichloromethane / Cooling
4: tetrakis(triphenylphosphine) palladium(0); sodium formate; N-ethyl-N,N-diisopropylamine / acetonitrile / 4 h / 60 °C / Inert atmosphere
With
pyridine; copper(l) iodide; tetrakis(triphenylphosphine) palladium(0); hydroxylamine hydrochloride; tetrabutylammomium bromide; sodium formate; triethylamine; N-ethyl-N,N-diisopropylamine;
In
dichloromethane; N,N-dimethyl-formamide; acetonitrile;
4: amino-Heck reaction;
DOI:10.1055/s-0030-1259556
- Guidance literature:
-
Multi-step reaction with 2 steps
1: triethylamine / dichloromethane / Cooling
2: tetrakis(triphenylphosphine) palladium(0); sodium formate; N-ethyl-N,N-diisopropylamine / acetonitrile / 4 h / 60 °C / Inert atmosphere
With
tetrakis(triphenylphosphine) palladium(0); sodium formate; triethylamine; N-ethyl-N,N-diisopropylamine;
In
dichloromethane; acetonitrile;
2: amino-Heck reaction;
DOI:10.1055/s-0030-1259556
