5,6-bis-p-(benzyloxy)benzoyloxy-4,7-di(p-(tert-butyldimethylsilyloxy)phenyl)benzo[d][1,3]dioxole

Base Information

• Chemical Name: 5,6-bis-p-(benzyloxy)benzoyloxy-4,7-di(p-(tert-butyldimethylsilyloxy)phenyl)benzo[d][1,3]dioxole
• CAS No.: 1160726-23-7
• Molecular Formula: C₅₉H₆₂O₁₀Si₂
• Molecular Weight: 987.306

Synonyms:5,6-bis-p-(benzyloxy)benzoyloxy-4,7-di(p-(tert-butyldimethylsilyloxy)phenyl)benzo[d][1,3]dioxole

Chemical Property of 5,6-bis-p-(benzyloxy)benzoyloxy-4,7-di(p-(tert-butyldimethylsilyloxy)phenyl)benzo[d][1,3]dioxole

Chemical Property:

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Technology Process of 5,6-bis-p-(benzyloxy)benzoyloxy-4,7-di(p-(tert-butyldimethylsilyloxy)phenyl)benzo[d][1,3]dioxole

There total 1 articles about 5,6-bis-p-(benzyloxy)benzoyloxy-4,7-di(p-(tert-butyldimethylsilyloxy)phenyl)benzo[d][1,3]dioxole which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

C31H42O6Si2 (956024-19-4) + 4-(benzyloxy)benzoic acid chloride (1486-50-6) → 5,6-bis-p-(benzyloxy)benzoyloxy-4,7-di(p-(tert-butyldimethylsilyloxy)phenyl)benzo[d][1,3]dioxole (1160726-23-7)

Guidance literature:

C₃₁H₄₂O₆Si₂; With n-butyllithium; In tetrahydrofuran; hexane; at -78 ℃; for 0.25h; Inert atmosphere;

4-(benzyloxy)benzoic acid chloride; In tetrahydrofuran; hexane; at -78 - 20 ℃; Inert atmosphere;

DOI:10.1021/jo900638b

Reference yield: 85.0%

5,6-bis-p-(benzyloxy)benzoyloxy-4,7-di(p-(tert-butyldimethylsilyloxy)phenyl)benzo[d][1,3]dioxole (1160726-23-7) + lead(IV) tetraacetate (546-67-8) → 5,6-bis-p-(benzyloxy)benzoyloxy-4,7-di(p-(tert-butyldimethylsilyloxy)phenyl)benzo[d][1,3]dioxol-2-yl acetate (1160726-24-8)

Guidance literature:

In benzene; at 80 ℃; for 20h; Inert atmosphere;

DOI:10.1021/jo900638b

upstream raw materials:

C₃₁H₄₂O₆Si₂

4-(benzyloxy)benzoic acid chloride

Downstream raw materials:

5,6-bis-p-(benzyloxy)benzoyloxy-4,7-di(p-(tert-butyldimethylsilyloxy)phenyl)benzo[d][1,3]dioxol-2-yl acetate

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