3-benzyloxycarbonyl-7-ethoxycarbonyl-1,6-dimethyl-3,7-diazatricyclo<4.1.0.0^2,5>heptane

Base Information

• Chemical Name: 3-benzyloxycarbonyl-7-ethoxycarbonyl-1,6-dimethyl-3,7-diazatricyclo<4.1.0.0^2,5>heptane
• CAS No.: 113730-69-1
• Molecular Formula: C₂₄H₂₆N₂O₄
• Molecular Weight: 406.481

Synonyms:3-benzyloxycarbonyl-7-ethoxycarbonyl-1,6-dimethyl-3,7-diazatricyclo<4.1.0.0^2,5>heptane

Chemical Property of 3-benzyloxycarbonyl-7-ethoxycarbonyl-1,6-dimethyl-3,7-diazatricyclo<4.1.0.0^2,5>heptane

Chemical Property:

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Technology Process of 3-benzyloxycarbonyl-7-ethoxycarbonyl-1,6-dimethyl-3,7-diazatricyclo<4.1.0.0^2,5>heptane

There total 5 articles about 3-benzyloxycarbonyl-7-ethoxycarbonyl-1,6-dimethyl-3,7-diazatricyclo<4.1.0.0^2,5>heptane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 30.0%

n-ethoxycarbonyl-p-nitrobenzene sulfonamide (22818-81-1) + 2-benzyloxycarbonyl-5,6-dimethyl-2-azabicyclo<2.2.0>hex-5-ene (106895-29-8,113775-90-9) → 3-benzyloxycarbonyl-7-ethoxycarbonyl-1,6-dimethyl-3,7-diazatricyclo<4.1.0.02,5>heptane (113730-69-1)

Guidance literature:

With benzyltriethylammonium bromide; sodium hydrogencarbonate; In dichloromethane; water; for 5h; Ambient temperature;

Reference yield:

3,4-Lutidin (583-58-4) → 3-benzyloxycarbonyl-7-ethoxycarbonyl-1,6-dimethyl-3,7-diazatricyclo<4.1.0.02,5>heptane (113730-69-1)

Guidance literature:

Multi-step reaction with 3 steps

1: tetrahydrofuran / 2 h / -5 °C

2: CH₂Cl₂ / 22 h / Irradiation

3: 30 percent / benzyltriethylammonium bromide, NaHCO₃ (0.5N) / CH₂Cl₂; H₂O / 5 h / Ambient temperature

With benzyltriethylammonium bromide; sodium hydrogencarbonate; In tetrahydrofuran; dichloromethane; water;

Reference yield:

phenylmagnesium bromide → 3-benzyloxycarbonyl-7-ethoxycarbonyl-1,6-dimethyl-3,7-diazatricyclo<4.1.0.02,5>heptane (113730-69-1)

Guidance literature:

Multi-step reaction with 3 steps

1: tetrahydrofuran / 2 h / -5 °C

2: CH₂Cl₂ / 22 h / Irradiation

3: 30 percent / benzyltriethylammonium bromide, NaHCO₃ (0.5N) / CH₂Cl₂; H₂O / 5 h / Ambient temperature

With benzyltriethylammonium bromide; sodium hydrogencarbonate; In tetrahydrofuran; dichloromethane; water;

upstream raw materials:

n-ethoxycarbonyl-p-nitrobenzene sulfonamide

2-benzyloxycarbonyl-5,6-dimethyl-2-azabicyclo<2.2.0>hex-5-ene

3,4-Lutidin

benzyl chloroformate

Downstream raw materials:

2,4-Dimethyl-7-phenyl-3,6-diaza-tricyclo[3.2.0.0^2,4]heptane-3-carboxylic acid ethyl ester

2,4-Dimethyl-7-phenyl-3,6-diaza-tricyclo[3.2.0.0^2,4]hept-6-ene-3-carboxylic acid ethyl ester

2,7-Dimethyl-5-phenyl-[1,4]diazepine-1-carboxylic acid ethyl ester

1-ethoxycarbonyl-6,7-dimethyl-4-phenyl-1,3-diazepine

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