Technology Process of 2-(3-isopropenylphenyl)propan-1-ol
There total 1 articles about 2-(3-isopropenylphenyl)propan-1-ol which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
1,3-bis(1-methylethenyl)-benzene;
With
dimethylsulfide borane complex;
In
tetrahydrofuran;
at 0 - 20 ℃;
With
sodium hydroxide; dihydrogen peroxide;
In
tetrahydrofuran;
DOI:10.1016/S0957-4166(02)00202-1
- Guidance literature:
-
Multi-step reaction with 4 steps
1.1: 98 percent / H2 / 5 percent Pd/C / ethyl acetate
2.1: Porcine pancreatic lipase / various solvent(s) / 96 h / 20 °C
2.2: KOH / methanol
2.3: Porcine pancreatic lipase / various solvent(s) / 48 h / 20 °C
3.1: 4-toluenesulfonyl chloride / pyridine / 0 °C
3.2: 62 percent / dimethylsulfoxide / 1 h / 50 °C
4.1: 75 percent / diisobutylaluminium hydride / tetrahydrofuran / -10 - 20 °C
With
porcine pancreatic lipase; hydrogen; diisobutylaluminium hydride; p-toluenesulfonyl chloride;
palladium on activated charcoal; 5% Pd on active carbon;
In
tetrahydrofuran; pyridine; ethyl acetate;
DOI:10.1016/S0957-4166(02)00202-1
