(3aS,7aS)-1-benzyl-3a,4,5,6,7,7a-hexahydro-3a-(3',4'-methylenedioxyphenyl)-6-oxoindoline

Base Information

Chemical Name:(3aS*,7aS*)-1-benzyl-3a,4,5,6,7,7a-hexahydro-3a-(3',4'-methylenedioxyphenyl)-6-oxoindoline
CAS No.:32209-88-4
Molecular Formula:C₂₂H₂₃NO₃
Molecular Weight:349.43
Hs Code.:

Synonyms:(3aS*,7aS*)-1-benzyl-3a,4,5,6,7,7a-hexahydro-3a-(3',4'-methylenedioxyphenyl)-6-oxoindoline

Suppliers and Price of (3aS*,7aS*)-1-benzyl-3a,4,5,6,7,7a-hexahydro-3a-(3',4'-methylenedioxyphenyl)-6-oxoindoline

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of (3aS*,7aS*)-1-benzyl-3a,4,5,6,7,7a-hexahydro-3a-(3',4'-methylenedioxyphenyl)-6-oxoindoline

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Technology Process of (3aS*,7aS*)-1-benzyl-3a,4,5,6,7,7a-hexahydro-3a-(3',4'-methylenedioxyphenyl)-6-oxoindoline

There total 7 articles about (3aS*,7aS*)-1-benzyl-3a,4,5,6,7,7a-hexahydro-3a-(3',4'-methylenedioxyphenyl)-6-oxoindoline which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 29.0%

: 78-94-4,25038-87-3
methyl vinyl ketone

: 32042-34-5
(1-benzo[1,3]dioxol-5-yl-cyclopropylmethylene)-benzyl-amine

: 32209-88-4
(3aS*,7aS*)-1-benzyl-3a,4,5,6,7,7a-hexahydro-3a-(3',4'-methylenedioxyphenyl)-6-oxoindoline

Guidance literature:: With benzylamine hydrochloride; sodium sulfate; In acetonitrile; for 5h; Heating / reflux;

Reference yield:

: 114047-02-8
2-allyl-5,5-ethylenedioxy-2-(3',4'-methylenedioxyphenyl)cyclohexanol

: 32209-88-4
(3aS*,7aS*)-1-benzyl-3a,4,5,6,7,7a-hexahydro-3a-(3',4'-methylenedioxyphenyl)-6-oxoindoline

Guidance literature:: Multi-step reaction with 3 steps

1: 256 mg

2: 87.4 percent / osmium tetroxide (OsO₄), sodium metaperiodate (NaIO₄) / dioxane; H₂O

3: 1.) K₂CO₃, NaBH₄; 2.) HCl (10percent) / 1.) MeOH, room temp., 3 h; 2.) reflux, 0.5 h

With hydrogenchloride; sodium tetrahydroborate; sodium periodate; osmium(VIII) oxide; potassium carbonate; In 1,4-dioxane; water;

Reference yield:

: 114046-99-0
8-Allyl-8-benzo[1,3]dioxol-5-yl-1,4-dioxa-spiro[4.5]decan-7-one

: 32209-88-4
(3aS*,7aS*)-1-benzyl-3a,4,5,6,7,7a-hexahydro-3a-(3',4'-methylenedioxyphenyl)-6-oxoindoline

Guidance literature:: Multi-step reaction with 4 steps

1: 79 percent / sodium borohydride (NaBH₄) / methanol / 2 h / Ambient temperature

2: 256 mg

3: 87.4 percent / osmium tetroxide (OsO₄), sodium metaperiodate (NaIO₄) / dioxane; H₂O

4: 1.) K₂CO₃, NaBH₄; 2.) HCl (10percent) / 1.) MeOH, room temp., 3 h; 2.) reflux, 0.5 h

With hydrogenchloride; sodium tetrahydroborate; sodium periodate; osmium(VIII) oxide; potassium carbonate; In 1,4-dioxane; methanol; water;