4-Methyl-N-[(R)-2-oxo-1-((4S,5R,4'R)-2,2,2',2'-tetramethyl-[4,4']bi[[1,3]dioxolanyl]-5-yl)-ethyl]-benzenesulfonamide

Base Information

Chemical Name:4-Methyl-N-[(R)-2-oxo-1-((4S,5R,4'R)-2,2,2',2'-tetramethyl-[4,4']bi[[1,3]dioxolanyl]-5-yl)-ethyl]-benzenesulfonamide
CAS No.:91414-44-7
Molecular Formula:C₁₉H₂₇NO₇S
Molecular Weight:413.492
Hs Code.:

Synonyms:4-Methyl-N-[(R)-2-oxo-1-((4S,5R,4'R)-2,2,2',2'-tetramethyl-[4,4']bi[[1,3]dioxolanyl]-5-yl)-ethyl]-benzenesulfonamide

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Chemical Property of 4-Methyl-N-[(R)-2-oxo-1-((4S,5R,4'R)-2,2,2',2'-tetramethyl-[4,4']bi[[1,3]dioxolanyl]-5-yl)-ethyl]-benzenesulfonamide

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Technology Process of 4-Methyl-N-[(R)-2-oxo-1-((4S,5R,4'R)-2,2,2',2'-tetramethyl-[4,4']bi[[1,3]dioxolanyl]-5-yl)-ethyl]-benzenesulfonamide

There total 3 articles about 4-Methyl-N-[(R)-2-oxo-1-((4S,5R,4'R)-2,2,2',2'-tetramethyl-[4,4']bi[[1,3]dioxolanyl]-5-yl)-ethyl]-benzenesulfonamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 79.0%

: 91414-38-9
2-deoxy-3,4:5,6-di-O-isopropylidene-2-p-toluenesulfonamido-D-glucose diethyl dithioacetal

: 91414-44-7
4-Methyl-N-[(R)-2-oxo-1-((4S,5R,4'R)-2,2,2',2'-tetramethyl-[4,4']bi[[1,3]dioxolanyl]-5-yl)-ethyl]-benzenesulfonamide

Guidance literature:: With cadmium(II) carbonate; mercury dichloride; In water; acetone; for 14h; Ambient temperature;
DOI:10.1016/0008-6215(84)85080-6

Reference yield:

: 91414-35-6
2-(toluene-4-sulfonylamino)-2-deoxy-D-glucose-diethyldithioacetal

: 91414-44-7
4-Methyl-N-[(R)-2-oxo-1-((4S,5R,4'R)-2,2,2',2'-tetramethyl-[4,4']bi[[1,3]dioxolanyl]-5-yl)-ethyl]-benzenesulfonamide

Guidance literature:: Multi-step reaction with 2 steps

1: 88 percent / cc. H₂SO₄ / acetone / 2 h / Ambient temperature

2: 79 percent / HgCl₂, CdCO₃ / acetone; H₂O / 14 h / Ambient temperature

With cadmium(II) carbonate; sulfuric acid; mercury dichloride; In water; acetone;
DOI:10.1016/0008-6215(84)85080-6

Reference yield:

: 109010-47-1
2-deoxy-2-p-toluenesulfonamido-D-glucopyranose

: 91414-44-7
4-Methyl-N-[(R)-2-oxo-1-((4S,5R,4'R)-2,2,2',2'-tetramethyl-[4,4']bi[[1,3]dioxolanyl]-5-yl)-ethyl]-benzenesulfonamide

Guidance literature:: Multi-step reaction with 3 steps

1: 75 percent / zinc chloride / 36 h / Ambient temperature

2: 88 percent / cc. H₂SO₄ / acetone / 2 h / Ambient temperature

3: 79 percent / HgCl₂, CdCO₃ / acetone; H₂O / 14 h / Ambient temperature

With cadmium(II) carbonate; sulfuric acid; mercury dichloride; zinc(II) chloride; In water; acetone;
DOI:10.1016/0008-6215(84)85080-6