3--1-propanol

Base Information

• Chemical Name: 3--1-propanol
• CAS No.: 125289-66-9
• Molecular Formula: C₁₄H₂₀O₂
• Molecular Weight: 220.312

Synonyms:3--1-propanol

Chemical Property of 3--1-propanol

Chemical Property:

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Technology Process of 3--1-propanol

There total 7 articles about 3--1-propanol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 84.0%

3-(4-hydroxyphenyl)propan-1-ol (10210-17-0) + prenyl bromide (870-63-3) → 3--1-propanol (125289-66-9)

Guidance literature:

With potassium carbonate; In acetone; for 1h; Reflux;

DOI:10.1016/j.bmcl.2012.03.057

Reference yield: 36.0%

3-methyl-2-butenyl 3-[4-(3-methyl-2-butenyloxy)-phenyl]propyl ether (410087-93-3) → 3--1-propanol (125289-66-9)

Guidance literature:

With 2,3-dicyano-5,6-dichloro-p-benzoquinone; In dichloromethane; water; at 20 ℃; for 2h;

DOI:10.1055/s-2002-20480

Reference yield: 26.0%

3-methyl-2-butenyl 3-[4-(3-methyl-2-butenyloxy)-phenyl]propyl ether (410087-93-3) → 3-[4-hydroxy-3-(3-methyl-2-butenyl)phenyl]propanol (13515-57-6) + 3--1-propanol (125289-66-9) + 6-(3-hydroxypropyl)-3,4-dihydro-2,2-dimethyl-3-iodo-2H-1-benzopyran (410087-97-7) + 4-[3-[(3-methyl-2-butenyl)oxy]propyl]phenol (477290-19-0)

Guidance literature:

With iodine; In dichloromethane; at 0 - 20 ℃; for 2h;

DOI:10.1016/S0040-4020(02)00539-2

upstream raw materials:

ethyl 3-[4-(3-methyl-but-2-enyloxy)phenyl]-propionate

3-methyl-2-butenyl 3-[4-(3-methyl-2-butenyloxy)-phenyl]propyl ether

3-(4-hydroxyphenyl)propan-1-ol

3-(4-hydroxy-phenyl)-propionic acid ethyl ester

Downstream raw materials:

4-[4-(3-hydroxy-propyl)-phenoxy]-2-methyl-but-2-en-1-ol

3--1-propanol

(E)-3--1-propanol

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