5,5'-bis(4,6-dimethoxy-2,3-diphenyl-1H-indol-7-yl)-2,2'-bi-(1,3,4-oxadiazole)

Base Information

Chemical Name:5,5'-bis(4,6-dimethoxy-2,3-diphenyl-1H-indol-7-yl)-2,2'-bi-(1,3,4-oxadiazole)
CAS No.:1569643-08-8
Molecular Formula:C₄₈H₃₆N₆O₆
Molecular Weight:792.85
Hs Code.:

Synonyms:5,5'-bis(4,6-dimethoxy-2,3-diphenyl-1H-indol-7-yl)-2,2'-bi-(1,3,4-oxadiazole)

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Chemical Property of 5,5'-bis(4,6-dimethoxy-2,3-diphenyl-1H-indol-7-yl)-2,2'-bi-(1,3,4-oxadiazole)

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Technology Process of 5,5'-bis(4,6-dimethoxy-2,3-diphenyl-1H-indol-7-yl)-2,2'-bi-(1,3,4-oxadiazole)

There total 4 articles about 5,5'-bis(4,6-dimethoxy-2,3-diphenyl-1H-indol-7-yl)-2,2'-bi-(1,3,4-oxadiazole) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 64.0%

: 1569642-86-9
N,N′-bis(4,6-dimethoxy-2,3-diphenyl-1H-indole-7-carbonyl)oxalohydrazide

: 1569643-08-8
5,5'-bis(4,6-dimethoxy-2,3-diphenyl-1H-indol-7-yl)-2,2'-bi-(1,3,4-oxadiazole)

Guidance literature:: With sodium hydroxide; trichlorophosphate; In ethyl acetate; for 24h; Reflux;
DOI:10.1016/j.bmc.2014.01.025

Reference yield:

: 1569642-67-6
4,6-dimethoxy-2,3-diphenyl-1H-indole-7-carbohydrazide

: 1569643-08-8
5,5'-bis(4,6-dimethoxy-2,3-diphenyl-1H-indol-7-yl)-2,2'-bi-(1,3,4-oxadiazole)

Guidance literature:: Multi-step reaction with 2 steps

1: triethylamine / dichloromethane / 1.5 h / 20 °C

2: trichlorophosphate; sodium hydroxide / ethyl acetate / 24 h / Reflux

With triethylamine; sodium hydroxide; trichlorophosphate; In dichloromethane; ethyl acetate;
DOI:10.1016/j.bmc.2014.01.025

Reference yield:

: 91107-10-7
4,6-dimethoxy-2,3-diphenyl-1H-indole

: 1569643-08-8
5,5'-bis(4,6-dimethoxy-2,3-diphenyl-1H-indol-7-yl)-2,2'-bi-(1,3,4-oxadiazole)

Guidance literature:: Multi-step reaction with 4 steps

1: 1,2-dichloro-ethane / 3 h / Reflux

2: hydrazine hydrate; triethylamine / acetonitrile / 1 h / 20 °C

3: triethylamine / dichloromethane / 1.5 h / 20 °C

4: trichlorophosphate; sodium hydroxide / ethyl acetate / 24 h / Reflux

With hydrazine hydrate; triethylamine; sodium hydroxide; trichlorophosphate; In dichloromethane; ethyl acetate; 1,2-dichloro-ethane; acetonitrile;
DOI:10.1016/j.bmc.2014.01.025