Technology Process of C21H20F4O6S2
There total 7 articles about C21H20F4O6S2 which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
C27H24F4O7S2;
With
tetra-(n-butyl)ammonium iodide;
In
tetrahydrofuran;
for 1.5h;
Heating / reflux;
sodium methansulfinate;
In
tetrahydrofuran;
for 18h;
Heating / reflux;
- Guidance literature:
-
Multi-step reaction with 2 steps
1: triethylamine
2: tetra-(n-butyl)ammonium iodide / tetrahydrofuran
With
tetra-(n-butyl)ammonium iodide; triethylamine;
In
tetrahydrofuran;
DOI:10.1016/j.bmcl.2012.11.047
- Guidance literature:
-
Multi-step reaction with 10 steps
1: potassium tert-butylate / tetrahydrofuran
2: Dess-Martin periodane / dichloromethane
3: trimethylsilyl trifluoromethanesulfonate
4: 3-chloro-benzenecarboperoxoic acid / dichloromethane
5: boron trifluoride diethyl etherate / dichloromethane
6: triethylamine / dichloromethane
7: potassium tert-butylate / tetrahydrofuran
8: ozone / dichloromethane
9: triethylamine
10: tetra-(n-butyl)ammonium iodide / tetrahydrofuran
With
trimethylsilyl trifluoromethanesulfonate; boron trifluoride diethyl etherate; potassium tert-butylate; tetra-(n-butyl)ammonium iodide; Dess-Martin periodane; ozone; triethylamine; 3-chloro-benzenecarboperoxoic acid;
In
tetrahydrofuran; dichloromethane;
DOI:10.1016/j.bmcl.2012.11.047