4,4,5,5-tetramethyl-2-(2-(4-(trifluoromethyl)phenyl)ethynyl)-1,3,2-dioxaborolane

Base Information

Chemical Name:4,4,5,5-tetramethyl-2-(2-(4-(trifluoromethyl)phenyl)ethynyl)-1,3,2-dioxaborolane
CAS No.:958633-18-6
Molecular Formula:C₁₅H₁₆BF₃O₂
Molecular Weight:296.097
Hs Code.:

Synonyms:4,4,5,5-tetramethyl-2-(2-(4-(trifluoromethyl)phenyl)ethynyl)-1,3,2-dioxaborolane

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Chemical Property of 4,4,5,5-tetramethyl-2-(2-(4-(trifluoromethyl)phenyl)ethynyl)-1,3,2-dioxaborolane

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Technology Process of 4,4,5,5-tetramethyl-2-(2-(4-(trifluoromethyl)phenyl)ethynyl)-1,3,2-dioxaborolane

There total 6 articles about 4,4,5,5-tetramethyl-2-(2-(4-(trifluoromethyl)phenyl)ethynyl)-1,3,2-dioxaborolane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 87.0%

: 705-31-7
4-trifluoromethylphenylacetylene

: 25015-63-8
4,4,5,5-tetramethyl-[1,3,2]-dioxaboralane

: 958633-18-6
4,4,5,5-tetramethyl-2-(2-(4-(trifluoromethyl)phenyl)ethynyl)-1,3,2-dioxaborolane

Guidance literature:: With 1,4-diaza-bicyclo[2.2.2]octane; iron(II) triflate; In toluene; at 100 ℃; for 24h; chemoselective reaction; Inert atmosphere; Schlenk technique;
DOI:10.1002/adsc.201800588

Reference yield: 81.0%

: 61676-62-8
2-Isopropoxy-4,4,5,5-tetramethyl-1,3,2-dioxaborolane

: 705-31-7
4-trifluoromethylphenylacetylene

: 958633-18-6
4,4,5,5-tetramethyl-2-(2-(4-(trifluoromethyl)phenyl)ethynyl)-1,3,2-dioxaborolane

Guidance literature:: With C₁₅H₁₄N₄; caesium carbonate; triphenylphosphine; silver(I) chloride; In N,N-dimethyl-formamide; at 50 ℃; for 24h; Inert atmosphere; Schlenk technique;
DOI:10.1016/j.tet.2014.06.033

Reference yield:

: 76-09-5
2,3-dimethyl-2,3-butane diol

: 1086138-68-2
C₁₀H₇BO₃

: 705-31-7
4-trifluoromethylphenylacetylene

: 958633-18-6
4,4,5,5-tetramethyl-2-(2-(4-(trifluoromethyl)phenyl)ethynyl)-1,3,2-dioxaborolane

Guidance literature:: C₁₀H₇BO₃; 4-trifluoromethylphenylacetylene; With 2-Mercapto-1-methylimidazole; In toluene; at 110 ℃; for 18h;

2,3-dimethyl-2,3-butane diol; at 20 ℃; for 1h;
DOI:10.1021/acscatal.0c02682