N-benzoyl-α-D-galactofuranosylamide

Base Information

Chemical Name:N-benzoyl-α-D-galactofuranosylamide
CAS No.:1296128-99-8
Molecular Formula:C₁₃H₁₇NO₆
Molecular Weight:283.281
Hs Code.:

Synonyms:N-benzoyl-α-D-galactofuranosylamide

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Chemical Property of N-benzoyl-α-D-galactofuranosylamide

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Technology Process of N-benzoyl-α-D-galactofuranosylamide

There total 3 articles about N-benzoyl-α-D-galactofuranosylamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 62.0%

: 1097731-84-4
2-(diphenylphosphano)phenyl benzoate

: β-D-galactofuranosyl azide

: 1296128-99-8
N-benzoyl-α-D-galactofuranosylamide

Guidance literature:: 2-(diphenylphosphano)phenyl benzoate; β-D-galactofuranosyl azide; In 1,3-dimethyl-3,4,5,6-tetrahydro-2(1H)-pyrimidinone; N,N-dimethyl acetamide; at 70 ℃; for 4h;

With water; In 1,3-dimethyl-3,4,5,6-tetrahydro-2(1H)-pyrimidinone; N,N-dimethyl acetamide; at 70 ℃; for 2h; stereoselective reaction;
DOI:10.1016/j.carres.2010.12.020

Reference yield:

: 2,3,5,6-tetra-O-acetyl-β-D-galactofuranosyl azide

: 1296128-99-8
N-benzoyl-α-D-galactofuranosylamide

Guidance literature:: Multi-step reaction with 2 steps

1.1: sodium methylate / methanol / 1 h / 20 °C / Inert atmosphere

2.1: 1,3-dimethyl-3,4,5,6-tetrahydro-2(1H)-pyrimidinone; N,N-dimethyl acetamide / 4 h / 70 °C

2.2: 2 h / 70 °C

With sodium methylate; In methanol; 1,3-dimethyl-3,4,5,6-tetrahydro-2(1H)-pyrimidinone; N,N-dimethyl acetamide; 1.1: Zemplen deacetylation / 2.1: Staudinger reaction;
DOI:10.1016/j.carres.2010.12.020

Reference yield:

: 5531-53-3,10535-09-8,22435-12-7,40031-23-0,55123-31-4,62181-82-2,72002-47-2,72691-27-1,72691-28-2
1,2,3,5,6-penta-O-acetyl-β-D-galactofuranose

: 1296128-99-8
N-benzoyl-α-D-galactofuranosylamide

Guidance literature:: Multi-step reaction with 3 steps

1.1: trimethylsilylazide; tin(IV) chloride / dichloromethane / 24 h / 20 °C / Inert atmosphere

2.1: sodium methylate / methanol / 1 h / 20 °C / Inert atmosphere

3.1: 1,3-dimethyl-3,4,5,6-tetrahydro-2(1H)-pyrimidinone; N,N-dimethyl acetamide / 4 h / 70 °C

3.2: 2 h / 70 °C

With trimethylsilylazide; sodium methylate; tin(IV) chloride; In methanol; 1,3-dimethyl-3,4,5,6-tetrahydro-2(1H)-pyrimidinone; dichloromethane; N,N-dimethyl acetamide; 2.1: Zemplen deacetylation / 3.1: Staudinger reaction;
DOI:10.1016/j.carres.2010.12.020