1-(9,9,10,10,11,11,12,12,13,13,14,14,15,15,16,16,16-heptadecafluorohexadecyl)-4-iodobenzene

Base Information

Chemical Name:1-(9,9,10,10,11,11,12,12,13,13,14,14,15,15,16,16,16-heptadecafluorohexadecyl)-4-iodobenzene
CAS No.:1228259-63-9
Molecular Formula:C₂₂H₂₀F₁₇I
Molecular Weight:734.278
Hs Code.:

Synonyms:1-(9,9,10,10,11,11,12,12,13,13,14,14,15,15,16,16,16-heptadecafluorohexadecyl)-4-iodobenzene

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 1-(9,9,10,10,11,11,12,12,13,13,14,14,15,15,16,16,16-heptadecafluorohexadecyl)-4-iodobenzene

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Technology Process of 1-(9,9,10,10,11,11,12,12,13,13,14,14,15,15,16,16,16-heptadecafluorohexadecyl)-4-iodobenzene

There total 1 articles about 1-(9,9,10,10,11,11,12,12,13,13,14,14,15,15,16,16,16-heptadecafluorohexadecyl)-4-iodobenzene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 90.0%

: 1228259-81-1
1-bromo-4-(9,9,10,10,11,11,12,12,13,13,14,14,15,15,16,16,16-heptadecafluorohexadecyl)benzene

: 1228259-63-9
1-(9,9,10,10,11,11,12,12,13,13,14,14,15,15,16,16,16-heptadecafluorohexadecyl)-4-iodobenzene

Guidance literature:: With iodine; nickel; potassium iodide; In N,N-dimethyl-formamide; Inert atmosphere; Heating;
DOI:10.1055/s-0029-1218667

Reference yield: 21.0%

: 1228259-63-9
1-(9,9,10,10,11,11,12,12,13,13,14,14,15,15,16,16,16-heptadecafluorohexadecyl)-4-iodobenzene

: 1066-54-2
trimethylsilylacetylene

: 1-(9,9,10,10,11,11,12,12,13,13,14,14,15,15,16,16,16-heptadecafluorohexadecyl)-4-{[4-(9,9,10,10,11,11,12,12,13,13,14,14,15,15,16,16,16-heptadecafluorohexadecyl)phenyl]ethynyl}benzene

Guidance literature:: With bis-triphenylphosphine-palladium(II) chloride; copper(l) iodide; water; 1,8-diazabicyclo[5.4.0]undec-7-ene; In tetrahydrofuran; Inert atmosphere; Heating;
DOI:10.1055/s-0029-1218667