BOC-D-GLU-OET DCHA

Base Information

• Chemical Name: BOC-D-GLU-OET DCHA
• CAS No.: 449171-15-7
• Molecular Formula: C12H21 N O6
• Molecular Weight: 275.302
• Mol file: 449171-15-7.mol

Synonyms:BOC-D-GLU-OET DCHA;BOC-D-GLU-OET · DCHA;Boc-D-Glu(OH)-O-Et;

Chemical Property of BOC-D-GLU-OET DCHA

Chemical Property:

• PSA: 101.93000
• LogP: 1.69850

Purity/Quality:

99% ^*data from raw suppliers

BOC-D-GLU-OETDCHA 95 ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of BOC-D-GLU-OET DCHA

There total 1 articles about BOC-D-GLU-OET DCHA which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

→ Boc-D-Glu-OEt (449171-15-7)

Guidance literature:

Reference yield:

Boc-D-Glu-OEt (449171-15-7) → (R)-2-((S)-4-amino-4-carboxybutanamido)pentanedioic acid (1116-22-9,4553-17-7,6729-93-7,6931-86-8)

Guidance literature:

Multi-step reaction with 3 steps

1.1: bromo-tris(1-pyrrolidinyl)phosphonium hexafluorophosphate; N-ethyl-N,N-diisopropylamine / N,N-dimethyl-formamide / 0.17 h / Flow reactor

1.2: Amberlyst A-21 / 0.33 h / Flow reactor

2.1: sodium hydroxide; methanol / 3 h / 20 °C

3.1: trifluoroacetic acid / dichloromethane / 2 h / 0 - 20 °C

With methanol; N-ethyl-N,N-diisopropylamine; bromo-tris(1-pyrrolidinyl)phosphonium hexafluorophosphate; trifluoroacetic acid; sodium hydroxide; In dichloromethane; N,N-dimethyl-formamide;

DOI:10.1016/j.tet.2016.11.025

Reference yield:

Boc-D-Glu-OEt (449171-15-7) + methyl (2S)-2-amino-3-phenylpropanoate hydrochloride (7524-50-7) → (R)-ethyl 2-(tert-butoxycarbonylamino)-5-((S)-1-methoxy-1-oxo-3-phenylpropan-2-ylamino)-5-oxopentanoate

Guidance literature:

methyl (2S)-2-amino-3-phenylpropanoate hydrochloride; With N-ethyl-N,N-diisopropylamine; bromo-tris(1-pyrrolidinyl)phosphonium hexafluorophosphate; In N,N-dimethyl-formamide; for 0.166667h; Flow reactor;

Boc-D-Glu-OEt; In N,N-dimethyl-formamide; for 0.333333h; Flow reactor;

DOI:10.1016/j.tet.2016.11.025

Downstream raw materials:

(R)-2-((S)-4-amino-4-carboxybutanamido)pentanedioic acid

(R)-2-amino-5-(carboxymethylamino)-5-oxopentanoic acid

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