3S-3-amino-2-[(1-methylcyclohexanecarbonyl)amino]propionic acid tert-butyl ester

Base Information

Chemical Name:3S-3-amino-2-[(1-methylcyclohexanecarbonyl)amino]propionic acid tert-butyl ester
CAS No.:948092-69-1
Molecular Formula:C₁₅H₂₈N₂O₃
Molecular Weight:284.399
Hs Code.:

Synonyms:3S-3-amino-2-[(1-methylcyclohexanecarbonyl)amino]propionic acid tert-butyl ester

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Chemical Property of 3S-3-amino-2-[(1-methylcyclohexanecarbonyl)amino]propionic acid tert-butyl ester

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Technology Process of 3S-3-amino-2-[(1-methylcyclohexanecarbonyl)amino]propionic acid tert-butyl ester

There total 3 articles about 3S-3-amino-2-[(1-methylcyclohexanecarbonyl)amino]propionic acid tert-butyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 84.0%

: 948092-67-9
C₁₆H₂₈N₂O₄

: 948092-69-1
3S-3-amino-2-[(1-methylcyclohexanecarbonyl)amino]propionic acid tert-butyl ester

Guidance literature:: With pyridine; bis-[(trifluoroacetoxy)iodo]benzene; In acetonitrile;
DOI:10.1021/jm070002v

Reference yield:

: 1123-25-7
1-methyl-1-cyclohexanecarboxylic acid

: 948092-69-1
3S-3-amino-2-[(1-methylcyclohexanecarbonyl)amino]propionic acid tert-butyl ester

Guidance literature:: Multi-step reaction with 2 steps

1: 78 percent / 4-pyrrolidinopyridine; O-benzotriazole-N,N,N',N'-tetramethyluronium*PF₆; diisopropylethylamine / CH₂Cl₂ / 5 h / 20 °C

2: 84 percent / phenyliodine(III) bis(trifluoroacetate); pyridine / acetonitrile

With pyridine; 4-pyrrolidin-1-ylpyridine; N-ethyl-N,N-diisopropylamine; bis-[(trifluoroacetoxy)iodo]benzene; In dichloromethane; acetonitrile; 2: Hofmann rearrangement;
DOI:10.1021/jm070002v

Reference yield:

: 25456-86-4
L-asparagine tert-butyl ester

: 948092-69-1
3S-3-amino-2-[(1-methylcyclohexanecarbonyl)amino]propionic acid tert-butyl ester

Guidance literature:: Multi-step reaction with 2 steps

1: 78 percent / 4-pyrrolidinopyridine; O-benzotriazole-N,N,N',N'-tetramethyluronium*PF₆; diisopropylethylamine / CH₂Cl₂ / 5 h / 20 °C

2: 84 percent / phenyliodine(III) bis(trifluoroacetate); pyridine / acetonitrile

With pyridine; 4-pyrrolidin-1-ylpyridine; N-ethyl-N,N-diisopropylamine; bis-[(trifluoroacetoxy)iodo]benzene; In dichloromethane; acetonitrile; 2: Hofmann rearrangement;
DOI:10.1021/jm070002v