({2-[2,4-Dioxo-5-phenyl-3-(3-phenyl-ureido)-2,3,4,5-tetrahydro-benzo[b][1,4]diazepin-1-yl]-acetyl}-phenyl-amino)-acetic acid ethyl ester

Base Information

• Chemical Name: ({2-[2,4-Dioxo-5-phenyl-3-(3-phenyl-ureido)-2,3,4,5-tetrahydro-benzo[b][1,4]diazepin-1-yl]-acetyl}-phenyl-amino)-acetic acid ethyl ester
• CAS No.: 173908-72-0
• Molecular Formula: C₃₄H₃₁N₅O₆
• Molecular Weight: 605.65

Synonyms:({2-[2,4-Dioxo-5-phenyl-3-(3-phenyl-ureido)-2,3,4,5-tetrahydro-benzo[b][1,4]diazepin-1-yl]-acetyl}-phenyl-amino)-acetic acid ethyl ester

Chemical Property of ({2-[2,4-Dioxo-5-phenyl-3-(3-phenyl-ureido)-2,3,4,5-tetrahydro-benzo[b][1,4]diazepin-1-yl]-acetyl}-phenyl-amino)-acetic acid ethyl ester

Chemical Property:

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Technology Process of ({2-[2,4-Dioxo-5-phenyl-3-(3-phenyl-ureido)-2,3,4,5-tetrahydro-benzo[b][1,4]diazepin-1-yl]-acetyl}-phenyl-amino)-acetic acid ethyl ester

There total 9 articles about ({2-[2,4-Dioxo-5-phenyl-3-(3-phenyl-ureido)-2,3,4,5-tetrahydro-benzo[b][1,4]diazepin-1-yl]-acetyl}-phenyl-amino)-acetic acid ethyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

N-phenylglycine ethyl ester (2216-92-4) → ({2-[2,4-Dioxo-5-phenyl-3-(3-phenyl-ureido)-2,3,4,5-tetrahydro-benzo[b][1,4]diazepin-1-yl]-acetyl}-phenyl-amino)-acetic acid ethyl ester (173908-72-0)

Guidance literature:

Multi-step reaction with 2 steps

1: Et₃N / CH₂Cl₂ / Ambient temperature

2: 1.) NaH / 1.) DMF, 30 min, 2.) DMF, RT, 16 h

With sodium hydride; triethylamine; In dichloromethane;

DOI:10.1021/jm950626d

Reference yield:

phenyl isocyanate (103-71-9) → ({2-[2,4-Dioxo-5-phenyl-3-(3-phenyl-ureido)-2,3,4,5-tetrahydro-benzo[b][1,4]diazepin-1-yl]-acetyl}-phenyl-amino)-acetic acid ethyl ester (173908-72-0)

Guidance literature:

Multi-step reaction with 2 steps

1: 72 percent / CH₂Cl₂ / 2 h / Ambient temperature

2: 1.) NaH / 1.) DMF, 30 min, 2.) DMF, RT, 16 h

With sodium hydride; In dichloromethane;

DOI:10.1021/jm950626d

Reference yield:

3-amino-1-phenyl-1,5-dihydrobenzo<1,4>diazepine-2,4-dione (153930-38-2) → ({2-[2,4-Dioxo-5-phenyl-3-(3-phenyl-ureido)-2,3,4,5-tetrahydro-benzo[b][1,4]diazepin-1-yl]-acetyl}-phenyl-amino)-acetic acid ethyl ester (173908-72-0)

Guidance literature:

Multi-step reaction with 2 steps

1: 72 percent / CH₂Cl₂ / 2 h / Ambient temperature

2: 1.) NaH / 1.) DMF, 30 min, 2.) DMF, RT, 16 h

With sodium hydride; In dichloromethane;

DOI:10.1021/jm950626d

upstream raw materials:

1-(2,4-dioxo-1-phenyl-2,3,4,5-tetrahydro-1H-benzo<1,4>diazepin-3-yl)-3-phenylurea

N-phenylglycine ethyl ester

phenyl isocyanate

3-amino-1-phenyl-1,5-dihydrobenzo<1,4>diazepine-2,4-dione

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