[5,15-bis(benzenebiuret)-10,20-bis(4-octylphenyl)porphyrinato]zinc(II)

Base Information

Chemical Name:[5,15-bis(benzenebiuret)-10,20-bis(4-octylphenyl)porphyrinato]zinc(II)
CAS No.:1393353-66-6
Molecular Formula:C₆₄H₆₆N₁₀O₄Zn
Molecular Weight:1104.68
Hs Code.:

Synonyms:[5,15-bis(benzenebiuret)-10,20-bis(4-octylphenyl)porphyrinato]zinc(II)

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Chemical Property of [5,15-bis(benzenebiuret)-10,20-bis(4-octylphenyl)porphyrinato]zinc(II)

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Technology Process of [5,15-bis(benzenebiuret)-10,20-bis(4-octylphenyl)porphyrinato]zinc(II)

There total 5 articles about [5,15-bis(benzenebiuret)-10,20-bis(4-octylphenyl)porphyrinato]zinc(II) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 41.0%

: 1097967-23-1
4-pinacolatoboronic ester-benzenebiuret

: 1403955-27-0
C₄₈H₅₀Br₂N₄Zn

: 1393353-66-6
[5,15-bis(benzenebiuret)-10,20-bis(4-octylphenyl)porphyrinato]zinc(II)

Guidance literature:: With tetrakis(triphenylphosphine) palladium⁽⁰⁾; potassium carbonate; In tetrahydrofuran; water; for 48h; Inert atmosphere; Reflux;
DOI:10.1039/c2cc33438k

Reference yield: 41.0%

: 1097967-23-1
4-pinacolatoboronic ester-benzenebiuret

: 1173502-37-8
[5,15-bis(4-octylphenyl)porphyrinato]zinc(II)

: 1393353-66-6
[5,15-bis(benzenebiuret)-10,20-bis(4-octylphenyl)porphyrinato]zinc(II)

Guidance literature:: With catalyst:Pd(PPh₃)4, K₂CO₃; NBS; In tetrahydrofuran; methanol; dichloromethane; Zn complex reacted with NBS in CH2Cl2/CH3OH, reacted with boron compoundin THF catalized by Pd(PPh3)4/K2CO3;
DOI:10.1039/c2cc33438k

Reference yield:

: 49763-66-8
4-octylbenzaldehyde

: 1393353-66-6
[5,15-bis(benzenebiuret)-10,20-bis(4-octylphenyl)porphyrinato]zinc(II)

Guidance literature:: Multi-step reaction with 4 steps

1.1: trifluoroacetic acid / dichloromethane / 16 h / 20 °C / Inert atmosphere; Darkness

1.2: 2 h / Inert atmosphere

2.1: zinc diacetate / methanol / 3 h / 60 °C / Inert atmosphere

3.1: N-Bromosuccinimide / methanol; dichloromethane / 0.17 h / 0 °C / Inert atmosphere

4.1: tetrakis(triphenylphosphine) palladium⁽⁰⁾; potassium carbonate / tetrahydrofuran; water / 48 h / Inert atmosphere; Reflux

With N-Bromosuccinimide; tetrakis(triphenylphosphine) palladium⁽⁰⁾; zinc diacetate; potassium carbonate; trifluoroacetic acid; In tetrahydrofuran; methanol; dichloromethane; water;
DOI:10.1039/c2cc33438k