C₃₆H₅₆O₇Si₃

Base Information

Chemical Name:C₃₆H₅₆O₇Si₃
CAS No.:1350623-73-2
Molecular Formula:C₃₆H₅₆O₇Si₃
Molecular Weight:685.093
Hs Code.:

C<sub>36</sub>H<sub>56</sub>O<sub>7</sub>Si<sub>3</sub>

Synonyms:C₃₆H₅₆O₇Si₃

Suppliers and Price of C₃₆H₅₆O₇Si₃

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 0 raw suppliers

Chemical Property of C₃₆H₅₆O₇Si₃

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of C₃₆H₅₆O₇Si₃

There total 14 articles about C₃₆H₅₆O₇Si₃ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 98.0%

: 1350623-71-0
C₂₄H₂₈O₇Si

: 69739-34-0
t-butyldimethylsiyl triflate

: 1350623-73-2
C₃₆H₅₆O₇Si₃

Guidance literature:: C₂₄H₂₈O₇Si; With triethylamine; In diethyl ether; at 0 ℃; for 0.5h; Inert atmosphere;

t-butyldimethylsiyl triflate; In diethyl ether; at -5 ℃; for 0.833333h; Inert atmosphere;
DOI:10.1021/ol2028256

Reference yield:

: C₃₆H₆₆O₅Si₃

: 1350623-73-2
C₃₆H₅₆O₇Si₃

Guidance literature:: Multi-step reaction with 8 steps

1.1: trifluoroacetic acid / dichloromethane / 24 h / 0 - 20 °C / Molecular sieve; Inert atmosphere

2.1: pyridine hydrogenfluoride / tetrahydrofuran / 4.8 h / -5 °C

3.1: 1-hydroxy-3H-benz[d][1,2]iodoxole-1,3-dione / dimethyl sulfoxide / 9.6 h / 20 °C / Inert atmosphere

4.1: zinc(II) chloride / tetrahydrofuran; diethyl ether / 0.25 h / -78 °C / Inert atmosphere

4.2: 0.75 h / -78 °C / Inert atmosphere

5.1: trifluoroacetic acid / diethyl ether / 10 h / 0 °C

6.1: pyridine hydrogenfluoride / tetrahydrofuran / 0 °C

7.1: tributylphosphine / acetonitrile / -40 °C / Inert atmosphere

8.1: triethylamine / diethyl ether / 0.5 h / 0 °C / Inert atmosphere

8.2: 0.83 h / -5 °C / Inert atmosphere

With tributylphosphine; pyridine hydrogenfluoride; triethylamine; trifluoroacetic acid; zinc(II) chloride; 1-hydroxy-3H-benz[d][1,2]iodoxole-1,3-dione; In tetrahydrofuran; diethyl ether; dichloromethane; dimethyl sulfoxide; acetonitrile;
DOI:10.1021/ol2028256

Reference yield:

: 343338-29-4
1,2-dideoxy-3,6-di-O-triisopropylsilyl-2-deoxy-D-arabino-1-hexenopyranose

: 1350623-73-2
C₃₆H₅₆O₇Si₃

Guidance literature:: Multi-step reaction with 11 steps

1.1: tetra-(n-butyl)ammonium iodide; sodium hydride / N,N-dimethyl-formamide / 2.5 h / 0 °C / Inert atmosphere

2.1: triphenylphosphine hydrobromide / dichloromethane; water / 13.97 h / 0 - 20 °C

3.1: sodium acetate; pyridinium chlorochromate / dichloromethane / 1.5 h / 20 °C / Molecular sieve; Inert atmosphere

4.1: lithium trimethylsilylacetylenide / tetrahydrofuran; hexane / 0.88 h / -78 °C / Inert atmosphere

5.1: pyridine hydrogenfluoride / tetrahydrofuran / 4.8 h / -5 °C

6.1: 1-hydroxy-3H-benz[d][1,2]iodoxole-1,3-dione / dimethyl sulfoxide / 9.6 h / 20 °C / Inert atmosphere

7.1: zinc(II) chloride / tetrahydrofuran; diethyl ether / 0.25 h / -78 °C / Inert atmosphere

7.2: 0.75 h / -78 °C / Inert atmosphere

8.1: trifluoroacetic acid / diethyl ether / 10 h / 0 °C

9.1: pyridine hydrogenfluoride / tetrahydrofuran / 0 °C

10.1: tributylphosphine / acetonitrile / -40 °C / Inert atmosphere

11.1: triethylamine / diethyl ether / 0.5 h / 0 °C / Inert atmosphere

11.2: 0.83 h / -5 °C / Inert atmosphere

With tributylphosphine; lithium trimethylsilylacetylenide; sodium acetate; triphenylphosphine hydrobromide; tetra-(n-butyl)ammonium iodide; sodium hydride; pyridine hydrogenfluoride; triethylamine; pyridinium chlorochromate; trifluoroacetic acid; zinc(II) chloride; 1-hydroxy-3H-benz[d][1,2]iodoxole-1,3-dione; In tetrahydrofuran; diethyl ether; hexane; dichloromethane; water; dimethyl sulfoxide; N,N-dimethyl-formamide; acetonitrile;
DOI:10.1021/ol2028256