N-(4-azido-2,6-diisopropylphenyl)-N′-(2,6-diisopropylphenyl) imidazolinium chloride

Base Information

Chemical Name:N-(4-azido-2,6-diisopropylphenyl)-N′-(2,6-diisopropylphenyl) imidazolinium chloride
CAS No.:1604799-63-4
Molecular Formula:C₂₇H₃₈N₅*Cl
Molecular Weight:468.085
Hs Code.:

Synonyms:N-(4-azido-2,6-diisopropylphenyl)-N′-(2,6-diisopropylphenyl) imidazolinium chloride

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Chemical Property of N-(4-azido-2,6-diisopropylphenyl)-N′-(2,6-diisopropylphenyl) imidazolinium chloride

Chemical Property:

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Technology Process of N-(4-azido-2,6-diisopropylphenyl)-N′-(2,6-diisopropylphenyl) imidazolinium chloride

There total 5 articles about N-(4-azido-2,6-diisopropylphenyl)-N′-(2,6-diisopropylphenyl) imidazolinium chloride which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 88.0%

: N-(4-Azido-2,6-diisopropylphenyl)-N′-(2,6-diisopropylphenyl)ethane-1,2-diamine dihydrochloride

: 1604799-63-4
N-(4-azido-2,6-diisopropylphenyl)-N′-(2,6-diisopropylphenyl) imidazolinium chloride

Guidance literature:: With formic acid; orthoformic acid triethyl ester; In ethanol; for 2h; Reflux;
DOI:10.1039/c4dt00429a

Reference yield:

: 24544-04-5
2,6-diisopropylbenzenamine

: 1604799-63-4
N-(4-azido-2,6-diisopropylphenyl)-N′-(2,6-diisopropylphenyl) imidazolinium chloride

Guidance literature:: Multi-step reaction with 5 steps

1.1: toluene / 0.25 h / 0 °C

2.1: sodium carbonate / dichloromethane / 2 h / 20 °C

3.1: sodium tetrahydroborate; trifluoroborane diethyl ether / tetrahydrofuran / 2 h / 29 °C

4.1: sodium hydrogencarbonate / water

4.2: 3 h / 70 °C / Inert atmosphere

5.1: orthoformic acid triethyl ester; formic acid / ethanol / 2 h / Reflux

With sodium tetrahydroborate; formic acid; trifluoroborane diethyl ether; sodium hydrogencarbonate; sodium carbonate; orthoformic acid triethyl ester; In tetrahydrofuran; ethanol; dichloromethane; water; toluene;
DOI:10.1039/c4dt00429a

Reference yield:

: 1189374-17-1
N-(2,6-diisopropylphenyl)-N′-(4-iodo-2,6-diisopropylphenyl)oxalamide

: 1604799-63-4
N-(4-azido-2,6-diisopropylphenyl)-N′-(2,6-diisopropylphenyl) imidazolinium chloride

Guidance literature:: Multi-step reaction with 3 steps

1.1: sodium tetrahydroborate; trifluoroborane diethyl ether / tetrahydrofuran / 2 h / 29 °C

2.1: sodium hydrogencarbonate / water

2.2: 3 h / 70 °C / Inert atmosphere

3.1: orthoformic acid triethyl ester; formic acid / ethanol / 2 h / Reflux

With sodium tetrahydroborate; formic acid; trifluoroborane diethyl ether; sodium hydrogencarbonate; orthoformic acid triethyl ester; In tetrahydrofuran; ethanol; water;
DOI:10.1039/c4dt00429a