4-methyl-N-prop-2-ynyl-N-[5-(4-methoxy-2,6-dimethyl-phenyl)-furan-2yl-methyl]-benzenesulfonamide

Base Information

Chemical Name:4-methyl-N-prop-2-ynyl-N-[5-(4-methoxy-2,6-dimethyl-phenyl)-furan-2yl-methyl]-benzenesulfonamide
CAS No.:914661-87-3
Molecular Formula:C₂₄H₂₅NO₄S
Molecular Weight:423.533
Hs Code.:

Synonyms:4-methyl-N-prop-2-ynyl-N-[5-(4-methoxy-2,6-dimethyl-phenyl)-furan-2yl-methyl]-benzenesulfonamide

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Chemical Property of 4-methyl-N-prop-2-ynyl-N-[5-(4-methoxy-2,6-dimethyl-phenyl)-furan-2yl-methyl]-benzenesulfonamide

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Technology Process of 4-methyl-N-prop-2-ynyl-N-[5-(4-methoxy-2,6-dimethyl-phenyl)-furan-2yl-methyl]-benzenesulfonamide

There total 4 articles about 4-methyl-N-prop-2-ynyl-N-[5-(4-methoxy-2,6-dimethyl-phenyl)-furan-2yl-methyl]-benzenesulfonamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: [5-(4-methoxy-2,6-dimethyl-phenyl)-furan-2-ylmethyl]-prop-2-ynyl-amine

: 98-59-9
p-toluenesulfonyl chloride

: 914661-87-3
4-methyl-N-prop-2-ynyl-N-[5-(4-methoxy-2,6-dimethyl-phenyl)-furan-2yl-methyl]-benzenesulfonamide

Guidance literature:: With triethylamine; In dichloromethane; at 20 ℃; for 12h;
DOI:10.1002/chem.200600533

Reference yield:

: 914661-74-8
2-(4-methoxy-2,6-dimethyl-phenyl)-furan

: 914661-87-3
4-methyl-N-prop-2-ynyl-N-[5-(4-methoxy-2,6-dimethyl-phenyl)-furan-2yl-methyl]-benzenesulfonamide

Guidance literature:: Multi-step reaction with 4 steps

1: 96 percent / phosphorus oxychloride / 12 h / 40 °C

2: magnesium sulfate / CH₂Cl₂ / 24 h / 20 °C

3: sodium borohydride / methanol / 3 h / 20 °C

4: 920 mg / triethylamine / CH₂Cl₂ / 12 h / 20 °C

With sodium tetrahydroborate; magnesium sulfate; triethylamine; trichlorophosphate; In methanol; dichloromethane; 1: Vilsmeier-Haack reaction;
DOI:10.1002/chem.200600533

Reference yield:

: 914661-85-1
5-(4-methoxy-2,6-dimethyl-phenyl)-furan-2-carbaldehyde

: 914661-87-3
4-methyl-N-prop-2-ynyl-N-[5-(4-methoxy-2,6-dimethyl-phenyl)-furan-2yl-methyl]-benzenesulfonamide

Guidance literature:: Multi-step reaction with 3 steps

1: magnesium sulfate / CH₂Cl₂ / 24 h / 20 °C

2: sodium borohydride / methanol / 3 h / 20 °C

3: 920 mg / triethylamine / CH₂Cl₂ / 12 h / 20 °C

With sodium tetrahydroborate; magnesium sulfate; triethylamine; In methanol; dichloromethane;
DOI:10.1002/chem.200600533