cis-α-(4'-pyridylamino)methylenepropiophenone

Base Information

Chemical Name:cis-α-(4'-pyridylamino)methylenepropiophenone
CAS No.:77871-76-2
Molecular Formula:C₁₅H₁₄N₂O
Molecular Weight:238.289
Hs Code.:

Synonyms:cis-α-(4'-pyridylamino)methylenepropiophenone

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of cis-α-(4'-pyridylamino)methylenepropiophenone

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Technology Process of cis-α-(4'-pyridylamino)methylenepropiophenone

There total 1 articles about cis-α-(4'-pyridylamino)methylenepropiophenone which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 65.0%

: 504-24-5
4-aminopyridine

: 55439-08-2
3-Hydroxy-2-methyl-1-oxo-1-phenylprop-2-ene

: 77871-76-2
cis-α-(4'-pyridylamino)methylenepropiophenone

Guidance literature:: With piperidine; In ethanol; for 5h; Heating;

Reference yield: 95.0%

: 77871-76-2
cis-α-(4'-pyridylamino)methylenepropiophenone

: 72945-07-4
2-Methyl-1-phenyl-3-(4'-pyridylamino)propan-1-ol

Guidance literature:: With sodium tetrahydroborate; In ethanol; for 4h; Heating;

Reference yield:

: 77871-76-2
cis-α-(4'-pyridylamino)methylenepropiophenone

: 77871-82-0
3-Methyl-4-phenyl-[1,6]naphthyridine

Guidance literature:: Multi-step reaction with 3 steps

1: 95 percent / sodium borohydride / ethanol / 4 h / Heating

2: 65 percent / 70percent H₂SO₄ / 1) 1h, 0 deg C, 2) room temp.

3: 58 percent / 10percent Pd/C / 4 h / 200 °C

With sodium tetrahydroborate; sulfuric acid; palladium on activated charcoal; In ethanol;