3-Phenyl-2,3-dihydro-1-benzothiophenoxid

Base Information

• Chemical Name: 3-Phenyl-2,3-dihydro-1-benzothiophenoxid
• CAS No.: 10413-38-4
• Molecular Formula: C₁₄H₁₂O₂S
• Molecular Weight: 244.314

Synonyms:3-Phenyl-2,3-dihydro-1-benzothiophenoxid

Chemical Property of 3-Phenyl-2,3-dihydro-1-benzothiophenoxid

Chemical Property:

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Technology Process of 3-Phenyl-2,3-dihydro-1-benzothiophenoxid

There total 3 articles about 3-Phenyl-2,3-dihydro-1-benzothiophenoxid which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 90.0%

1,1-dioxo-3-phenylbenzothiophene (27183-55-7) → 3-Phenyl-2,3-dihydro-1-benzothiophenoxid (10413-38-4)

Guidance literature:

With hydrogen; palladium on activated charcoal; In acetic acid; at 35 ℃; for 0.25h;

Reference yield:

benzothiophene-1,1-dioxide (825-44-5) + phenylboronic acid (98-80-6) → 3-Phenyl-2,3-dihydro-1-benzothiophenoxid (10413-38-4)

Guidance literature:

With chloro(1,5-cyclooctadiene)rhodium(I) dimer; potassium hydroxide; In 1,4-dioxane; water; at 100 ℃; for 12h; Reagent/catalyst; Catalytic behavior; Inert atmosphere; Glovebox; Sealed tube;

DOI:10.1021/acs.orglett.0c04114

Reference yield:

→ 3-Phenyl-2,3-dihydro-1-benzothiophenoxid (10413-38-4)

Guidance literature:

<1>Benzothieno<2,3-b><1>benzothiophen-5,5-dioxid (III), Raney-Ni;

DOI:10.1016/S0040-4020(01)97837-8

upstream raw materials:

1,1-dioxo-3-phenylbenzothiophene

benzothiophene-1,1-dioxide

phenylboronic acid

Downstream raw materials:

2,3-dihydro-3-phenylbenzothiophen

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