trans-W(O-2,6-C₆H₃Me₂)4Cl₂

Base Information

Chemical Name:trans-W(O-2,6-C₆H₃Me₂)4Cl₂
CAS No.:82972-39-2
Molecular Formula:C₃₂H₃₆Cl₂O₄W
Molecular Weight:739.391
Hs Code.:

trans-W(O-2,6-C<sub>6</sub>H<sub>3</sub>Me<sub>2</sub>)4Cl<sub>2</sub>

Synonyms:trans-W(O-2,6-C₆H₃Me₂)4Cl₂

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Chemical Property of trans-W(O-2,6-C₆H₃Me₂)4Cl₂

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Technology Process of trans-W(O-2,6-C₆H₃Me₂)4Cl₂

There total 1 articles about trans-W(O-2,6-C₆H₃Me₂)4Cl₂ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 65.0%

: 576-26-1,25134-01-4
2.6-dimethylphenol

: 13283-01-7
tungsten(VI) chloride

: 82972-39-2
trans-W(O-2,6-C₆H₃Me₂)4Cl₂

Guidance literature:: In neat (no solvent); under N2; 0.252 mmol dimethylphenol and 0.0252 mmol WCl6 heated until the phenol melts; mixt. heated for 20 min; extn. with pentane to remove the phenol; recrystn. from CH2Cl2; elem. anal.;

Reference yield: 82.0%

: 82972-39-2
trans-W(O-2,6-C₆H₃Me₂)4Cl₂

: 99248-59-6
W(O-2,6-C₆H₃Me₂)4

Guidance literature:: With sodium amalgam; In diethyl ether; W compound added rapidly as solid to ether at -30°C contg. sodium amalgam (0.5%); soln. stirred for 2 h at 25°C; mixt. filtered, solvent removed in vac., residue extd. with ether; ether removed in vac.;