(1S,2R,6S,7R,10S)-10-Amino-1,7,8,9,10-pentamethyl-4-phenyl-4-aza-tricyclo[5.2.1.0^2,6]dec-8-ene-3,5-dione

Base Information

• Chemical Name: (1S,2R,6S,7R,10S)-10-Amino-1,7,8,9,10-pentamethyl-4-phenyl-4-aza-tricyclo[5.2.1.0^2,6]dec-8-ene-3,5-dione
• CAS No.: 114564-30-6
• Molecular Formula: C₂₀H₂₄N₂O₂
• Molecular Weight: 324.423

Synonyms:(1S,2R,6S,7R,10S)-10-Amino-1,7,8,9,10-pentamethyl-4-phenyl-4-aza-tricyclo[5.2.1.0^2,6]dec-8-ene-3,5-dione

Chemical Property of (1S,2R,6S,7R,10S)-10-Amino-1,7,8,9,10-pentamethyl-4-phenyl-4-aza-tricyclo[5.2.1.0^2,6]dec-8-ene-3,5-dione

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Technology Process of (1S,2R,6S,7R,10S)-10-Amino-1,7,8,9,10-pentamethyl-4-phenyl-4-aza-tricyclo[5.2.1.0^2,6]dec-8-ene-3,5-dione

There total 1 articles about (1S,2R,6S,7R,10S)-10-Amino-1,7,8,9,10-pentamethyl-4-phenyl-4-aza-tricyclo[5.2.1.0^2,6]dec-8-ene-3,5-dione which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 100.0%

N-phenyl-maleimide (941-69-5) + 1,2,3,4,5-Pentamethyl-cyclopenta-2,4-dienylamine (85739-52-2) → (1S,2R,6S,7R,10S)-10-Amino-1,7,8,9,10-pentamethyl-4-phenyl-4-aza-tricyclo[5.2.1.02,6]dec-8-ene-3,5-dione (114564-30-6)

Guidance literature:

In dichloromethane; at 22 ℃; for 3.5h;

DOI:10.1021/ja00159a038

Reference yield: 100.0%

(1S,2R,6S,7R,10S)-10-Amino-1,7,8,9,10-pentamethyl-4-phenyl-4-aza-tricyclo[5.2.1.02,6]dec-8-ene-3,5-dione (114564-30-6) + acetic anhydride (108-24-7) → N-((1S,2R,6S,7R,10S)-1,7,8,9,10-Pentamethyl-3,5-dioxo-4-phenyl-4-aza-tricyclo[5.2.1.02,6]dec-8-en-10-yl)-acetamide (114564-29-3,125277-86-3)

Guidance literature:

With pyridine; In dichloromethane; at 22 ℃; for 23h;

DOI:10.1021/ja00159a038

upstream raw materials:

N-phenyl-maleimide

1,2,3,4,5-Pentamethyl-cyclopenta-2,4-dienylamine

Downstream raw materials:

N-((1S,2R,6S,7R,10S)-1,7,8,9,10-Pentamethyl-3,5-dioxo-4-phenyl-4-aza-tricyclo[5.2.1.0^2,6]dec-8-en-10-yl)-acetamide

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