Technology Process of C18H20O4
There total 6 articles about C18H20O4 which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
With
phosphorus pentoxide; toluene-4-sulfonic acid;
In
toluene;
at 0 ℃;
DOI:10.1021/ol071085c
- Guidance literature:
-
Multi-step reaction with 4 steps
1: aq. K2CO3; Bu4NBr / 9 h / Heating
2: Cu; pyridine; H2O / 13 h / Heating
3: 1.36 g / LiAlH4 / tetrahydrofuran / 2 h / 20 °C
4: 92 percent / p-TsOH; P2O5 / toluene / 0 °C
With
pyridine; lithium aluminium tetrahydride; tetrabutylammomium bromide; water; phosphorus pentoxide; copper; potassium carbonate; toluene-4-sulfonic acid;
In
tetrahydrofuran; toluene;
DOI:10.1021/ol071085c
- Guidance literature:
-
Multi-step reaction with 3 steps
1: Cu; pyridine; H2O / 13 h / Heating
2: 1.36 g / LiAlH4 / tetrahydrofuran / 2 h / 20 °C
3: 92 percent / p-TsOH; P2O5 / toluene / 0 °C
With
pyridine; lithium aluminium tetrahydride; water; phosphorus pentoxide; copper; toluene-4-sulfonic acid;
In
tetrahydrofuran; toluene;
DOI:10.1021/ol071085c