2-(S)-(triphenylmethylamino)-3-<1-(triphenylmethyl)imidazol-4(5)-yl>propyl 4-iodobenzyl ether

Base Information

Chemical Name:2-(S)-(triphenylmethylamino)-3-<1-(triphenylmethyl)imidazol-4(5)-yl>propyl 4-iodobenzyl ether
CAS No.:223910-53-0
Molecular Formula:C₅₁H₄₄IN₃O
Molecular Weight:841.834
Hs Code.:

Synonyms:2-(S)-(triphenylmethylamino)-3-<1-(triphenylmethyl)imidazol-4(5)-yl>propyl 4-iodobenzyl ether

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Chemical Property of 2-(S)-(triphenylmethylamino)-3-<1-(triphenylmethyl)imidazol-4(5)-yl>propyl 4-iodobenzyl ether

Chemical Property:

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Technology Process of 2-(S)-(triphenylmethylamino)-3-<1-(triphenylmethyl)imidazol-4(5)-yl>propyl 4-iodobenzyl ether

There total 4 articles about 2-(S)-(triphenylmethylamino)-3-<1-(triphenylmethyl)imidazol-4(5)-yl>propyl 4-iodobenzyl ether which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 76-83-5
trityl chloride

: 223910-53-0
2-(S)-(triphenylmethylamino)-3-<1-(triphenylmethyl)imidazol-4(5)-yl>propyl 4-iodobenzyl ether

Guidance literature:: Multi-step reaction with 3 steps

1: 100 percent / Et₃N / acetonitrile / Ambient temperature

2: 1.) LiAlH₄, 2.) aq. NaOH / 1.) THF, 2.) THF, RT, 15 min

3: 1.) NaH / 1.) DMF, RT, 1 h, 2.) DMF

With sodium hydroxide; lithium aluminium tetrahydride; sodium hydride; triethylamine; In acetonitrile;
DOI:10.1021/jm980408v

Reference yield:

: 4467-54-3,5619-10-3,7389-87-9,18684-16-7,22888-60-4,32381-17-2,92742-29-5,100009-20-9
l-histidine methyl ester dihydrochloride

: 223910-53-0
2-(S)-(triphenylmethylamino)-3-<1-(triphenylmethyl)imidazol-4(5)-yl>propyl 4-iodobenzyl ether

Guidance literature:: Multi-step reaction with 3 steps

1: 100 percent / Et₃N / acetonitrile / Ambient temperature

2: 1.) LiAlH₄, 2.) aq. NaOH / 1.) THF, 2.) THF, RT, 15 min

3: 1.) NaH / 1.) DMF, RT, 1 h, 2.) DMF

With sodium hydroxide; lithium aluminium tetrahydride; sodium hydride; triethylamine; In acetonitrile;
DOI:10.1021/jm980408v

Reference yield:

: 22888-57-9
2-(S)-(triphenylmethylamino)-3-<1-(triphenylmethyl)imidazol-4(5)-yl>propanoic acid methyl ester ditrityl-L-histidine methyl ester

: 223910-53-0
2-(S)-(triphenylmethylamino)-3-<1-(triphenylmethyl)imidazol-4(5)-yl>propyl 4-iodobenzyl ether

Guidance literature:: Multi-step reaction with 2 steps

1: 1.) LiAlH₄, 2.) aq. NaOH / 1.) THF, 2.) THF, RT, 15 min

2: 1.) NaH / 1.) DMF, RT, 1 h, 2.) DMF

With sodium hydroxide; lithium aluminium tetrahydride; sodium hydride;
DOI:10.1021/jm980408v