4-(1-(4-(triisopropylsilyl)ethyn-2-ylphenyl)ethyn-2-yl)-N,N-dihexylaniline

Base Information

Chemical Name:4-(1-(4-(triisopropylsilyl)ethyn-2-ylphenyl)ethyn-2-yl)-N,N-dihexylaniline
CAS No.:1392008-61-5
Molecular Formula:C₃₇H₅₅NSi
Molecular Weight:541.936
Hs Code.:

Synonyms:4-(1-(4-(triisopropylsilyl)ethyn-2-ylphenyl)ethyn-2-yl)-N,N-dihexylaniline

Suppliers and Price of 4-(1-(4-(triisopropylsilyl)ethyn-2-ylphenyl)ethyn-2-yl)-N,N-dihexylaniline

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 4-(1-(4-(triisopropylsilyl)ethyn-2-ylphenyl)ethyn-2-yl)-N,N-dihexylaniline

Chemical Property:

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Technology Process of 4-(1-(4-(triisopropylsilyl)ethyn-2-ylphenyl)ethyn-2-yl)-N,N-dihexylaniline

There total 5 articles about 4-(1-(4-(triisopropylsilyl)ethyn-2-ylphenyl)ethyn-2-yl)-N,N-dihexylaniline which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 84.0%

: 1392008-60-4
4-(1-(4-bromophenyl)ethyn-2-yl)-N,N-dihexylaniline

: 89343-06-6
tris-iso-propylsilyl acetylene

: 1392008-61-5
4-(1-(4-(triisopropylsilyl)ethyn-2-ylphenyl)ethyn-2-yl)-N,N-dihexylaniline

Guidance literature:: With bis-triphenylphosphine-palladium(II) chloride; copper(l) iodide; triethylamine; In toluene; at 90 ℃; Inert atmosphere;
DOI:10.1039/c2ob25536g

Reference yield: 53.0%

: 391198-57-5
[2-(4-iodophenyl)ethynyl]triisopropylsilane

: 406491-06-3
N,N-dihexyl-4-ethynylaniline

: 1392008-61-5
4-(1-(4-(triisopropylsilyl)ethyn-2-ylphenyl)ethyn-2-yl)-N,N-dihexylaniline

Guidance literature:: With bis-triphenylphosphine-palladium(II) chloride; copper(l) iodide; triethylamine; In tetrahydrofuran; at 70 ℃; for 16h; Inert atmosphere;
DOI:10.1002/chem.201901047

Reference yield:

: 90134-09-1
N,N-dihexyl-4-iodobenzenamine

: 1392008-61-5
4-(1-(4-(triisopropylsilyl)ethyn-2-ylphenyl)ethyn-2-yl)-N,N-dihexylaniline

Guidance literature:: Multi-step reaction with 4 steps

1: copper(l) iodide; bis-triphenylphosphine-palladium(II) chloride; triethylamine / tetrahydrofuran / 20 °C / Inert atmosphere

2: tetrabutyl ammonium fluoride / tetrahydrofuran / 20 °C / Inert atmosphere

3: copper(l) iodide; bis-triphenylphosphine-palladium(II) chloride; triethylamine / tetrahydrofuran / 16 h / 20 °C / Inert atmosphere

4: copper(l) iodide; bis-triphenylphosphine-palladium(II) chloride; triethylamine / toluene / 90 °C / Inert atmosphere

With bis-triphenylphosphine-palladium(II) chloride; copper(l) iodide; tetrabutyl ammonium fluoride; triethylamine; In tetrahydrofuran; toluene;
DOI:10.1039/c2ob25536g