[2-[3-bromo-4-(triisopropylsilyloxy)-phenyl]-1-(triisopropylsilyloxymethyl)ethyl]tritylamine

Base Information

Chemical Name:[2-[3-bromo-4-(triisopropylsilyloxy)-phenyl]-1-(triisopropylsilyloxymethyl)ethyl]tritylamine
CAS No.:613223-69-1
Molecular Formula:C₄₆H₆₆BrNO₂Si₂
Molecular Weight:801.111
Hs Code.:

Synonyms:[2-[3-bromo-4-(triisopropylsilyloxy)-phenyl]-1-(triisopropylsilyloxymethyl)ethyl]tritylamine

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of [2-[3-bromo-4-(triisopropylsilyloxy)-phenyl]-1-(triisopropylsilyloxymethyl)ethyl]tritylamine

Chemical Property:

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Technology Process of [2-[3-bromo-4-(triisopropylsilyloxy)-phenyl]-1-(triisopropylsilyloxymethyl)ethyl]tritylamine

There total 3 articles about [2-[3-bromo-4-(triisopropylsilyloxy)-phenyl]-1-(triisopropylsilyloxymethyl)ethyl]tritylamine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 76-83-5
trityl chloride

: 613223-69-1
[2-[3-bromo-4-(triisopropylsilyloxy)-phenyl]-1-(triisopropylsilyloxymethyl)ethyl]tritylamine

Guidance literature:: Multi-step reaction with 3 steps

1: 100 percent / triethylamine / dimethylformamide / 3 h / 20 °C

2: 65 percent / NBS / dimethylformamide / 2.5 h / 20 °C

3: 100 percent / 1,8-diazabicyclo[5.4.0]undec-7-ene / CH₂Cl₂ / 0.75 h / 0 °C

With N-Bromosuccinimide; 1,8-diazabicyclo[5.4.0]undec-7-ene; triethylamine; In dichloromethane; N,N-dimethyl-formamide;
DOI:10.1021/ja0365330

Reference yield:

: 3417-91-2
L-tyrosine methyl ester HCl

: 613223-69-1
[2-[3-bromo-4-(triisopropylsilyloxy)-phenyl]-1-(triisopropylsilyloxymethyl)ethyl]tritylamine

Guidance literature:: Multi-step reaction with 3 steps

1: 100 percent / triethylamine / dimethylformamide / 3 h / 20 °C

2: 65 percent / NBS / dimethylformamide / 2.5 h / 20 °C

3: 100 percent / 1,8-diazabicyclo[5.4.0]undec-7-ene / CH₂Cl₂ / 0.75 h / 0 °C

With N-Bromosuccinimide; 1,8-diazabicyclo[5.4.0]undec-7-ene; triethylamine; In dichloromethane; N,N-dimethyl-formamide;
DOI:10.1021/ja0365330

Reference yield:

: 18621-06-2
N-trityl-L-tyrosine methyl ester

: 613223-69-1
[2-[3-bromo-4-(triisopropylsilyloxy)-phenyl]-1-(triisopropylsilyloxymethyl)ethyl]tritylamine

Guidance literature:: Multi-step reaction with 2 steps

1: 65 percent / NBS / dimethylformamide / 2.5 h / 20 °C

2: 100 percent / 1,8-diazabicyclo[5.4.0]undec-7-ene / CH₂Cl₂ / 0.75 h / 0 °C

With N-Bromosuccinimide; 1,8-diazabicyclo[5.4.0]undec-7-ene; In dichloromethane; N,N-dimethyl-formamide;
DOI:10.1021/ja0365330