methyl N-(2-bromo-4-methylphenyl)carbamate

Base Information

Chemical Name:methyl N-(2-bromo-4-methylphenyl)carbamate
CAS No.:540797-44-2
Molecular Formula:C₉H₁₀BrNO₂
Molecular Weight:244.088
Hs Code.:

Synonyms:methyl N-(2-bromo-4-methylphenyl)carbamate

Suppliers and Price of methyl N-(2-bromo-4-methylphenyl)carbamate

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

American Custom Chemicals Corporation
METHYL N-(2-BROMO-4-METHYLPHENYL)CARBAMATE 95.00%
5G
$ 1295.03

American Custom Chemicals Corporation
METHYL N-(2-BROMO-4-METHYLPHENYL)CARBAMATE 95.00%
2.5G
$ 1065.66

American Custom Chemicals Corporation
METHYL N-(2-BROMO-4-METHYLPHENYL)CARBAMATE 95.00%
1G
$ 765.23

AK Scientific
MethylN-(2-bromo-4-methylphenyl)carbamate
100mg
$ 172.00

Total 1 raw suppliers

Chemical Property of methyl N-(2-bromo-4-methylphenyl)carbamate

Chemical Property:

Purity/Quality:: METHYL N-(2-BROMO-4-METHYLPHENYL)CARBAMATE 95.00% ^*data from reagent suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

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Technology Process of methyl N-(2-bromo-4-methylphenyl)carbamate

There total 3 articles about methyl N-(2-bromo-4-methylphenyl)carbamate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 88.0%

: 5602-96-0
methyl p-tolylcarbamate

: 540797-44-2
methyl N-(2-bromo-4-methylphenyl)carbamate

Guidance literature:: With N-Bromosuccinimide; palladium diacetate; toluene-4-sulfonic acid; In 1,2-dichloro-ethane; at 60 ℃; for 3h; Reagent/catalyst; Temperature; Solvent; regioselective reaction; Catalytic behavior; Sealed tube;
DOI:10.1021/acs.joc.6b00329

Reference yield:

2-bromo-p-toluidine: 583-68-6
2-bromo-p-toluidine

: 79-22-1
methyl chloroformate

: 540797-44-2
methyl N-(2-bromo-4-methylphenyl)carbamate

Guidance literature:: In ethyl acetate; at 80 ℃;
DOI:10.1016/j.tetlet.2013.07.037

Reference yield:

: 619-55-6
para-methylbenzamide

: 540797-44-2
methyl N-(2-bromo-4-methylphenyl)carbamate

Guidance literature:: Multi-step reaction with 2 steps

1: N-Bromosuccinimide; potassium tert-butylate / 0.67 h / 80 °C

2: N-Bromosuccinimide; toluene-4-sulfonic acid; palladium diacetate / 1,2-dichloro-ethane / 3 h / 60 °C / Sealed tube

With N-Bromosuccinimide; potassium tert-butylate; palladium diacetate; toluene-4-sulfonic acid; In 1,2-dichloro-ethane;
DOI:10.1021/acs.joc.6b00329