Bromdiethinyl-benzol

Base Information

Chemical Name:Bromdiethinyl-benzol
CAS No.:937-65-5
Molecular Formula:C₁₀H₅Br
Molecular Weight:205.054
Hs Code.:

Synonyms:Bromdiethinyl-benzol

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of Bromdiethinyl-benzol

Chemical Property:

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Technology Process of Bromdiethinyl-benzol

There total 1 articles about Bromdiethinyl-benzol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 935-14-8
1,4-diethynylbenzene

: 937-65-5
Bromdiethinyl-benzol

Guidance literature:: With N-Bromosuccinimide; silver nitrate; In acetone; at 20 ℃; for 3h;
DOI:10.1039/c0cc02156c

Reference yield: 83.0%

: ammonium thiocyanate

: 937-65-5
Bromdiethinyl-benzol

: (Z)-1-(2-bromo-1-thiocyanatovinyl)-4-ethynylbenzene

Guidance literature:: With Au-TiO₂; acetic acid; at 70 ℃; for 8h;
DOI:10.1021/acs.orglett.9b00728

Reference yield: 74.0%

: 937-65-5
Bromdiethinyl-benzol

: 1258403-31-4
1-((Z)-2-bromo-1-iodovinyl)-4-ethynylbenzene

Guidance literature:: With potassium iodide; In acetic anhydride; at 120 ℃; for 6h; optical yield given as %de; stereoselective reaction;
DOI:10.1039/c0cc02156c