2-benzyl-3-hydroxypropyl bromide

Base Information

Chemical Name:2-benzyl-3-hydroxypropyl bromide
CAS No.:1246953-53-6
Molecular Formula:C₁₀H₁₃BrO
Molecular Weight:229.117
Hs Code.:

Synonyms:2-benzyl-3-hydroxypropyl bromide

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Chemical Property of 2-benzyl-3-hydroxypropyl bromide

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Technology Process of 2-benzyl-3-hydroxypropyl bromide

There total 5 articles about 2-benzyl-3-hydroxypropyl bromide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 100.0%

: 129600-10-8
3-acetoxy-2-benzylpropyl bromide

: 1246953-53-6
2-benzyl-3-hydroxypropyl bromide

Guidance literature:: 3-acetoxy-2-benzylpropyl bromide; With diisobutylaluminium hydride; In tetrahydrofuran; hexane; at -78 ℃; for 1.75h; Inert atmosphere;

With water; In tetrahydrofuran; hexane; ethyl acetate;
DOI:10.1002/ejoc.201000539

Reference yield:

: 10317-12-1
3-benzyloxetane

: 1246953-53-6
2-benzyl-3-hydroxypropyl bromide

: C₁₀H₁₃BrO

Guidance literature:: 3-benzyloxetane; With 3-((3,5-bis(trifluoromethyl)phenyl)amino)-4-(((S)-3,3-dimethyl-1-((R)-2-methyl-2-(phenanthren-9-yl)pyrrolidin-1-yl)-1-oxobutan-2-yl)amino)cyclobut-3-ene-1,2-dione; In tert-butyl methyl ether; at -78 ℃; for 0.25h; Inert atmosphere;

With hydrogen bromide; In tert-butyl methyl ether; toluene; at -80 - -78 ℃; for 24h; Inert atmosphere;
DOI:10.1021/jacs.1c03992