Technology Process of C41H62O9Si
There total 5 articles about C41H62O9Si which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
With
potassium permanganate; sodium periodate;
In
aq. phosphate buffer; tert-butyl alcohol;
at 20 ℃;
for 1h;
pH=7.2;
Inert atmosphere;
DOI:10.1016/j.tet.2013.02.008
- Guidance literature:
-
Multi-step reaction with 2 steps
1: 1H-imidazole / tetrahydrofuran / 4 h / 20 °C
2: sodium periodate; potassium permanganate / tert-butyl alcohol; aq. phosphate buffer / 1 h / 20 °C / pH 7.2 / Inert atmosphere
With
1H-imidazole; potassium permanganate; sodium periodate;
In
tetrahydrofuran; aq. phosphate buffer; tert-butyl alcohol;
DOI:10.1016/j.tet.2013.02.008
- Guidance literature:
-
Multi-step reaction with 4 steps
1.1: 2,4,6-trichlorobenzoyl chloride; triethylamine / toluene / 3 h / 20 °C
1.2: 1.5 h / 50 °C
2.1: 2,3-dicyano-5,6-dichloro-p-benzoquinone / dichloromethane; water / 1 h / 20 °C
3.1: 1H-imidazole / tetrahydrofuran / 4 h / 20 °C
4.1: sodium periodate; potassium permanganate / tert-butyl alcohol; aq. phosphate buffer / 1 h / 20 °C / pH 7.2 / Inert atmosphere
With
1H-imidazole; potassium permanganate; sodium periodate; 2,4,6-trichlorobenzoyl chloride; triethylamine; 2,3-dicyano-5,6-dichloro-p-benzoquinone;
In
tetrahydrofuran; aq. phosphate buffer; dichloromethane; water; toluene; tert-butyl alcohol;
1.1: |Yamaguchi Lactonization / 1.2: |Yamaguchi Lactonization;
DOI:10.1016/j.tet.2013.02.008
