benzyl 4-(4-((R)-4-((1R,2S)-1-hydroxy-1-phenylpropan-2-ylamino)pentyl)phenyl)butylcarbamate

Base Information

Chemical Name:benzyl 4-(4-((R)-4-((1R,2S)-1-hydroxy-1-phenylpropan-2-ylamino)pentyl)phenyl)butylcarbamate
CAS No.:960398-54-3
Molecular Formula:C₃₂H₄₂N₂O₃
Molecular Weight:502.697
Hs Code.:

Synonyms:benzyl 4-(4-((R)-4-((1R,2S)-1-hydroxy-1-phenylpropan-2-ylamino)pentyl)phenyl)butylcarbamate

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Chemical Property of benzyl 4-(4-((R)-4-((1R,2S)-1-hydroxy-1-phenylpropan-2-ylamino)pentyl)phenyl)butylcarbamate

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Technology Process of benzyl 4-(4-((R)-4-((1R,2S)-1-hydroxy-1-phenylpropan-2-ylamino)pentyl)phenyl)butylcarbamate

There total 1 articles about benzyl 4-(4-((R)-4-((1R,2S)-1-hydroxy-1-phenylpropan-2-ylamino)pentyl)phenyl)butylcarbamate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 960398-80-5
benzyl 4-(4-(4-hydroxypentyl)phenyl)butylcarbamate

: 960398-54-3
benzyl 4-(4-((R)-4-((1R,2S)-1-hydroxy-1-phenylpropan-2-ylamino)pentyl)phenyl)butylcarbamate

: 960398-55-4
benzyl 4-(4-((S)-4-((1R,2S)-1-hydroxy-1-phenylpropan-2-ylamino)pentyl)phenyl)butylcarbamate

Guidance literature:: Multi-step reaction with 2 steps

1.1: 4 A molecular sieve; pyridinium chlorochromate / dichloromethane / 6 h / 20 °C

2.1: acetic acid / methanol / 1.5 h / 20 °C

2.2: 14 h / 20 °C

With 4 A molecular sieve; acetic acid; pyridinium chlorochromate; In methanol; dichloromethane;

Reference yield: 77.0%

: 960398-54-3
benzyl 4-(4-((R)-4-((1R,2S)-1-hydroxy-1-phenylpropan-2-ylamino)pentyl)phenyl)butylcarbamate

: 960398-56-5
(1R,2S)-2-((R)-5-(4-(4-aminobutyl)phenyl)pentan-2-ylamino)-1-phenylpropan-1-ol

Guidance literature:: With hydrogen; 10 % Pd(OH)2/C; In ethanol; at 20 ℃; for 66h; under 760.051 Torr;

Reference yield:

: 960398-54-3
benzyl 4-(4-((R)-4-((1R,2S)-1-hydroxy-1-phenylpropan-2-ylamino)pentyl)phenyl)butylcarbamate

: 3,5-diamino-6-chloro-N-(N-(4-(4-(((R)-4-(1R,2S)-1-hydroxy-1-phenylpropan-2-ylamno)pentyl)phenyl)butyl)carbamimidoyl)pyrazine-2-carboxamide

Guidance literature:: Multi-step reaction with 2 steps

1: hydrogen / 10 % Pd(OH)2/C / ethanol / 66 h / 20 °C / 760.05 Torr

2: N-ethyl-N,N-diisopropylamine / ethanol / 5.5 h / 75 °C

With hydrogen; N-ethyl-N,N-diisopropylamine; 10 % Pd(OH)2/C; In ethanol;