[5,15-bis(3-hydroxyphenyl)-10,20-bis(3,5-di-tert-butylphenyl)porphyrinato]zinc(II)

Base Information

• Chemical Name: [5,15-bis(3-hydroxyphenyl)-10,20-bis(3,5-di-tert-butylphenyl)porphyrinato]zinc(II)
• CAS No.: 1372607-71-0
• Molecular Formula: C₆₀H₆₀N₄O₂Zn
• Molecular Weight: 934.552

Synonyms:[5,15-bis(3-hydroxyphenyl)-10,20-bis(3,5-di-tert-butylphenyl)porphyrinato]zinc(II)

Chemical Property of [5,15-bis(3-hydroxyphenyl)-10,20-bis(3,5-di-tert-butylphenyl)porphyrinato]zinc(II)

Chemical Property:

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Technology Process of [5,15-bis(3-hydroxyphenyl)-10,20-bis(3,5-di-tert-butylphenyl)porphyrinato]zinc(II)

There total 1 articles about [5,15-bis(3-hydroxyphenyl)-10,20-bis(3,5-di-tert-butylphenyl)porphyrinato]zinc(II) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 98.0%

[5,15-bis(3-tert-butyldiphenylsiloxyphenyl)-10,20-bis(3,5-di-tert-butylphenyl)porphyrinato]zinc(II) (1372607-70-9) → [5,15-bis(3-hydroxyphenyl)-10,20-bis(3,5-di-tert-butylphenyl)porphyrinato]zinc(II) (1372607-71-0)

Guidance literature:

With methanol; cesium fluoride; In tetrahydrofuran; at 20 ℃; for 3h; Inert atmosphere;

DOI:10.1039/c2cc17568a

Reference yield: 99.0%

1,8-dibromooctane (4549-32-0) + [5,15-bis(3-hydroxyphenyl)-10,20-bis(3,5-di-tert-butylphenyl)porphyrinato]zinc(II) (1372607-71-0) → [5,15-bis(3-(1-bromooctanyloxy)phenyl)-10,20-bis(3,5-di-tert-butylphenyl)porphinato]zinc(II) (1372607-75-4)

Guidance literature:

With 18-crown-6 ether; potassium carbonate; In acetone; Inert atmosphere; Reflux;

DOI:10.1039/c2cc17568a

Reference yield: 98.0%

[5,15-bis(3-hydroxyphenyl)-10,20-bis(3,5-di-tert-butylphenyl)porphyrinato]zinc(II) (1372607-71-0) + bromopentene (1119-51-3) → C70H76N4O2Zn (1372607-72-1)

Guidance literature:

With 18-crown-6 ether; potassium carbonate; In tetrahydrofuran; Inert atmosphere; Reflux;

DOI:10.1039/c2cc17568a

upstream raw materials:

[5,15-bis(3-tert-butyldiphenylsiloxyphenyl)-10,20-bis(3,5-di-tert-butylphenyl)porphyrinato]zinc(II)

Downstream raw materials:

[5,15-bis(3-(1-bromooctanyloxy)phenyl)-10,20-bis(3,5-di-tert-butylphenyl)porphinato]zinc(II)

[5,15-bis(3-(1-butynyloxy)phenyl)-10,20-bis(3,5-di-tert-butylphenyl)porphyrinato]zinc(II)

C₇₀H₇₆N₄O₂Zn

C₁₃₆H₁₄₄N₈O₄Zn₂

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