ethyl (E)-3-chloro-4-[4'-hydroxy-3'-(2-methyl-1,3-dithian-2-yl)phenyl]cinnamate

Base Information

Chemical Name:ethyl (E)-3-chloro-4-[4'-hydroxy-3'-(2-methyl-1,3-dithian-2-yl)phenyl]cinnamate
CAS No.:1063713-14-3
Molecular Formula:C₂₉H₂₉ClO₃S₂
Molecular Weight:525.132
Hs Code.:

Synonyms:ethyl (E)-3-chloro-4-[4'-hydroxy-3'-(2-methyl-1,3-dithian-2-yl)phenyl]cinnamate

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of ethyl (E)-3-chloro-4-[4'-hydroxy-3'-(2-methyl-1,3-dithian-2-yl)phenyl]cinnamate

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Technology Process of ethyl (E)-3-chloro-4-[4'-hydroxy-3'-(2-methyl-1,3-dithian-2-yl)phenyl]cinnamate

There total 1 articles about ethyl (E)-3-chloro-4-[4'-hydroxy-3'-(2-methyl-1,3-dithian-2-yl)phenyl]cinnamate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 43.0%

: 524937-24-4
(E)-ethyl 3-(3-chloro-4-(trifluoromethylsulphonyloxy)phenyl)acrylate

: 1063713-13-2
3-(2-methyl-1,3-dithian-2-yl)-4-(t-butyldimethylsilyloxy)phenylboronic acid

: 1063713-14-3
ethyl (E)-3-chloro-4-[4'-hydroxy-3'-(2-methyl-1,3-dithian-2-yl)phenyl]cinnamate

Guidance literature:: With tetrakis(triphenylphosphine) palladium⁽⁰⁾; sodium carbonate; lithium chloride; In 1,2-dimethoxyethane; water; for 23h; Reflux; Inert atmosphere;
DOI:10.1021/jm800456k

Reference yield:

: 1063713-14-3
ethyl (E)-3-chloro-4-[4'-hydroxy-3'-(2-methyl-1,3-dithian-2-yl)phenyl]cinnamate

: 1063713-17-6
C₂₂H₂₃ClO₃S₂

Guidance literature:: ethyl (E)-3-chloro-4-[4'-hydroxy-3'-(2-methyl-1,3-dithian-2-yl)phenyl]cinnamate; With phosphorus tribromide; In dichloromethane; at -78 ℃;

With water; In dichloromethane;
DOI:10.1021/jm800456k